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In this study, the ligand functionalized nano-conjugate material was developed for the sensitive and selective detection and removal of toxic arsenic(V) and phosphate ions in aqueous media. The nano-conjugate material was fabricated based on the use of metal-organic frameworks with exhibited of high surface area, pore morphology, and tuneable shape. The newly design nano-conjugate material was exhibited the naked eye monitoring of the ultra-trace arsenic(V) and phosphate in a simple, fast, cost-effective and easy-to-use approach. The data clarified that the arsenic(V) and phosphate adsorption process were found to be relatively fast. The adsorption isotherms of arsenic(V) and phosphate from aqueous solutions to the nano-conjugate material were measured, and the results showed that the Langmuir isotherm was found to be the best represent the measured adsorption data. The maximum adsorption …