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Polypyrrole nanofiber/Zn-Fe layered double hydroxide (Ppy NF/Zn-Fe LDH) was synthesized as nanocomposite of enhanced adsorption and photocatalytic properties. The formation of the composite was confirmed by XRD, FT-IR, HSEM, HRTEM, BET surface area and UV-vis spectrophotometer. Ppy NF/Zn-Fe LDH composite exhibits clear enhancing in the specific surface area and obvious reducing in the band gap energy (from 2.8 eV for Zn-Fe LDH to 2.31 eV for the composite). This was reflected in a considerable improvement in the adsorption capacity and photocatalytic removal of safranin dye. The adsorption capacity was enhanced by about 22% higher than Ppy NF and by 31% higher than Zn-Fe LDH. The photocatalytic removal was improved by 41.6% higher than Ppy NF and by about 54% higher than Zn-Fe LDH. The adsorption of safranin dye by the composite is chemisorption adsorption and occurs in …