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The initiation and peak magmatic periods of the Emeishan Large Igneous Province (LIP) are well constrained by both biostratigraphic and radioisotopic dating methods; however, the age of cessation of volcanism is poorly constrained and continues to be debated. Marine carbonates interbedded with volcanic ashes across the Guadalupian–Lopingian boundary (GLB) are widespread in south China, and these ashes provide an opportunity to study its timing, origin, and potential relationship with the Emeishan LIP. Here we present biostratigraphic constraints, mineralogical and geochemical characteristics, and high-resolution geochronology of ash layers from the Maoershan and Chaotian sections. Stratigraphic correlation, especially conodont biostratigraphy, confines these ashes to the early Wuchiapingian. Those altered ashes are geochemically akin to alkali tonsteins from the coal seams of the lower …