作者
Nicholas J Brooks, Beatrice LLE Gauthe, Nick J Terrill, Sarah E Rogers, Richard H Templer, Oscar Ces, John M Seddon
发表日期
2010/6/1
期刊
Review of Scientific Instruments
卷号
81
期号
6
出版商
AIP Publishing
简介
A high pressure cell for small and wide-angle x-ray diffraction measurements of soft condensed matter samples has been developed, incorporating a fully automated pressure generating network. The system allows both static and pressure jump measurements in the range of 0.1–500 MPa. Pressure jumps can be performed as quickly as 5 ms, both with increasing and decreasing pressures. Pressure is generated by a motorized high pressure pump, and the system is controlled remotely via a graphical user interface to allow operation by a broad user base, many of whom may have little previous experience of high pressure technology. Samples are loaded through a dedicated port allowing the x-ray windows to remain in place throughout an experiment; this facilitates accurate subtraction of background scattering. The system has been designed specifically for use at beamline I22 at the Diamond Light Source …
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NJ Brooks, BLLE Gauthe, NJ Terrill, SE Rogers… - Review of Scientific Instruments, 2010