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This study aims to investigate phenolic compounds recovery from pistachio hull using cleaner production technology. The effects of solvent type (acetone, n-hexane, ethanol, methanol, and deionized water), solvent temperature (25, 50, 75 °C), and extraction time (0.5, 1, 2, 4, 8, 24 h) were optimized for maximum phenolic compounds extraction from the hull. The maximum phenolic compounds extraction (30.8 mg/g) was obtained for water at 75 °C temperature and 4 h extraction time. The pressure-driven membrane process was used to concentrate phenolic compounds from water used as a solvent. UP150, UP005, NF270, and NF90 membranes were used to concentrate the phenolic compounds. The contents of phenolic compounds in permeate and concentrate streams were determined by LC-MSMS. Moreover, the biopesticide properties of the recovered phenolic compounds were also investigated, which are …