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As more applications for nano-sized natural particles are discovered, simple, environmentally friendly ways to produce these particles become more important. This work prepares and characterizes nano-size bacterial cellulose particles using ultrasonication. Pellicle from nata de coco containing nanofibers was broken up in an electrical blender, then sonicated using an ultrasonic probe at 20 kHz and 3 W/mL for 30, 60 and 90 min. Transmission electron microscope observations indicate the particles become nano-sized after 60 min ultrasound. The maximum decomposition temperature before sonication was 373 °C, decreased to 357 °C after 60 min ultrasonication. Moisture absorption of the 90 min sonicated particles film is 60% slower compared to non-sonicated particles. After ultrasonication, the crystallinity index of the cellulose decreases. The functional groups of non-sonicated and sonicated …