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The bireforming of methane (CH₄) with carbon dioxide (CO₂) and water, called BRM, is a process for generating syngas, which is utilized as a feed for methanol production. The formation of multi-heterojunction by hybridizing cobalt aluminum lanthanum layered double hydroxide (CoAlLa-LDH), and TiO_{2Anatase/Rutile}@Ti₃C₂ MXene (TiO_2A/R@Ti₃C₂) with graphitic carbon nitride (g-C₃N₄) to form a g-C₃N₄/TiO_2A/R@Ti₃C₂/CoAlLa-LDH dual-S-scheme composite performed as an excellent candidate for photocatalytic BRM. The photocatalytic performance was studied for CO₂ dry reforming of methane (DRM), bireforming of methane (BRM), and CO₂ reduction with H₂O. The photocatalytic BRM was found to be an efficient reforming system with high-quality syngas production. The efficiency of the BRM process was then optimized by employing Response Surface Methodology (RSM). In RSM studies, it was …