Development and validation of LC-Q-TOF-MS methodology to determine mycotoxin biomarkers in human urine

N Dasí-Navarro, M Lozano, S Llop, A Esplugues… - Toxins, 2022 - mdpi.com
mycotoxins and their metabolites [36,37]. Liquid chromatography-mass spectrometry (LC-MS/MS)
is the method of choice for multi-mycotoxin … , finding DON-15-glucuronide and DON-3-…

Development of a sensitive and reliable UHPLC-MS/MS method for the determination of multiple urinary biomarkers of mycotoxin exposure

Z Liu, X Zhao, L Wu, S Zhou, Z Gong, Y Zhao, Y Wu - Toxins, 2020 - mdpi.com
Mycotoxins are toxic secondary metabolites produced under … analytical strategy represents
a reliable tool for mycotoxin … temperature and centrifuged at 6000 rpm for 15 min at 4 C. Fifty …

Dried urine spots as sampling technique for multi-mycotoxin analysis in human urine

J Schmidt, V Lindemann, M Olsen, B Cramer… - Mycotoxin …, 2021 - Springer
… -MS/MS based multi-mycotoxin analysis in human urine samples was developed by application
of dried urine … the analysis of mycotoxins and mycotoxin metabolites in urine samples by …

Mycotoxin analysis of human urine by LC-MS/MS: A comparative extraction study

L Escrivá, L Manyes, G Font, H Berrada - Toxins, 2017 - mdpi.com
… The lower mycotoxin levels detected in urine make the development of sensitive and … 4
/C18) and GC-MS/MS analysis to determine 15 mycotoxins and metabolites in human urine. The …

Assessing human exposure to pesticides and mycotoxins: optimization and validation of a method for multianalyte determination in urine samples

J Marín-Sáez, M Hernández-Mesa… - Analytical and …, 2024 - Springer
… In this study, an analytical method has been developed for … and mycotoxins, including their
most relevant metabolites, in … Then, samples were analysed by UHPLC-QqQ-MS/MS. Method …

Simultaneous detection of mycotoxins and pesticides in human urine samples: A 24-h diet intervention study comparing conventional and organic diets in Spain

JA Gallardo-Ramos, J Marín-Sáez, V Sanchis… - Food and Chemical …, 2024 - Elsevier
developed and validated for mycotoxins and pesticides in … the mycotoxins OTα and ENNB
and the non-specific metabolite … major mycotoxins and metabolites (eg aflatoxins B1, B2, 15-…

Sample preparation and mass spectrometry for determining mycotoxins, hazardous fungi, and their metabolites in the environment, food, and healthcare

Y Zhao, D Chen, H Duan, P Li, W Wu, X Wang… - TrAC Trends in …, 2023 - Elsevier
… in developing countries, causing mass death in mycotoxin-… For the detection of mycotoxins
with low volatility, GC-MS/MS helps to … mycotoxin exposure in humans, up to 10 human urine

Mycotoxins—Biomonitoring and human exposure

K Habschied, G Kanižai Šarić, V Krstanović… - Toxins, 2021 - mdpi.com
… of developing health problems, many of the stated mycotoxins … (3-AcDON), and 15-acetyldeoxynivalenol
(15-AcDON) are … in urine and its metabolites via the HPLC-MS/MS technique is …

High-throughput and sensitive determination of urinary zearalenone and metabolites by UPLC-MS/MS and its application to a human exposure study

C Li, C Deng, S Zhou, Y Zhao, D Wang, X Wang… - Analytical and …, 2018 - Springer
… -based strategies to assess human exposure to mycotoxinsHumans are easily exposed to
ZEN through their diet [15]. … studies have focused on developing LC-MS/MS methods that can …

[HTML][HTML] Ultra-sensitive, stable isotope assisted quantification of multiple urinary mycotoxin exposure biomarkers

B Šarkanj, CN Ezekiel, PC Turner, WA Abia… - Analytica chimica …, 2018 - Elsevier
… disease, mycotoxins and their metabolites are … development, validation, and critical
performance evaluation of the first SIDA-based UHPLC-MS/MS method for urinary multi-mycotoxin