Direct measurement of pregnanediol 3-glucuronide (PDG) in dried urine spots by liquid chromatography-mass spectrometry to detect ovulation
DJ Handelsman, R Nimmagadda, R Desai… - The Journal of Steroid …, 2021 - Elsevier
… The sensitivity (limit of detection (LOD) and limit of quantitation (LOQ) defined according to …
3 levels (accuracy and CV%) and extraction recovery (6 replicates at 3 levels on pooled urine …
3 levels (accuracy and CV%) and extraction recovery (6 replicates at 3 levels on pooled urine …
Quantitation of serum pregnanediol-3-glucuronide level in different endocrine statuses by LC–MS/MS
J Chen, H Hou, H Chen, Y Luo, Y He, H Wang… - … and biomedical analysis, 2020 - Elsevier
… and urine are frequently chosen as samples for clinical steroid hormone analysis, because of
their non-invasion (urine) … Blood/serum and urine are integrated biological fluids, which can …
their non-invasion (urine) … Blood/serum and urine are integrated biological fluids, which can …
Targeted LC–MS/MS analysis of steroid glucuronides in human urine
R Wang, MF Hartmann, SA Wudy - The Journal of Steroid Biochemistry and …, 2021 - Elsevier
… Only a very little amount of unconjugated testosterone was found in older children. The only
… for quantification of steroid glucuronides in human urine. The method was applied to urinary …
… for quantification of steroid glucuronides in human urine. The method was applied to urinary …
Longitudinal evaluation of multiple biomarkers for the detection of testosterone gel administration in women with normal menstrual cycle
… In females, T is produced in small amounts by the ovaries … in low urinary T levels, often
below the limit of quantification (… reference compounds (ERC) pregnanediol (PD) and 16-…
below the limit of quantification (… reference compounds (ERC) pregnanediol (PD) and 16-…
[HTML][HTML] Targeted metabolic profiling of urinary steroids with a focus on analytical accuracy and sample stability
N Vogg, T Müller, A Floren, T Dandekar… - Journal of Mass …, 2022 - Elsevier
… A method for the quantification of 11 deconjugated steroids (5-… , pregnanediol, and 5-pregnenediol)
in human urine was … for the quantification of a panel of 11 urinary steroids. We …
in human urine was … for the quantification of a panel of 11 urinary steroids. We …
A time-resolved fluorescence microsphere-lateral flow immunochromatographic strip for quantitative detection of Pregnanediol-3-glucuronide in urine samples
J Lin, S Li, B Ye, W Zheng, H Wang, Y Liu… - … in Bioengineering and …, 2023 - frontiersin.org
… detection. The current colloidal gold strips mostly detect ovulation by setting a detection …
The method developed in this paper achieved quantitative detection by using a fluorescent …
The method developed in this paper achieved quantitative detection by using a fluorescent …
Quantification of urinary steroids by supported liquid extraction with GC-MS/MS: Unravelling cyclic fluctuations of steroid profiling in regular menstrual cycle
M Liu, Y Ge, X Xu, L Liao - … of Pharmaceutical and Biomedical Analysis, 2022 - Elsevier
… The LLOQ was the lowest amount of an analyte that could be quantitatively determined
with acceptable precision (RSD ≤ 20%) and accuracy (recoveries between 80% and 120%). …
with acceptable precision (RSD ≤ 20%) and accuracy (recoveries between 80% and 120%). …
Development of the thin film solid phase microextraction (TF-SPME) method for metabolomics profiling of steroidal hormones from urine samples using LC-QTOF/MS
W Struck-Lewicka, B Karpińska, W Rodzaj… - Frontiers in Molecular …, 2023 - frontiersin.org
… The sensitivity enhancement is crucial in terms of extraction of trace amounts of compounds
or when there is a need for extraction of compounds at different concentration levels from …
or when there is a need for extraction of compounds at different concentration levels from …
… high performance liquid chromatography purification of underivatized urinary testosterone and metabolites for compound‐specific stable carbon isotope analysis
K Lalonde, A Barber, C Ayotte - Drug Testing and Analysis, 2021 - Wiley Online Library
… ERC is defined as pregnanediol (Pgdiol); … urinary matrix because during the analysis,
organic molecules transferred from the GC column to the combustion interface are quantitatively …
organic molecules transferred from the GC column to the combustion interface are quantitatively …
Reliability of a dried urine test for comprehensive assessment of urine hormones and metabolites
M Newman, DA Curran - BMC chemistry, 2021 - Springer
… , accuracy with small volumes, and ability to … ], as measurement of urinary ⍺-pregnanediol,
β-pregnanediol, estrone, and estradiol with this method are representative of both 24-h urine …
β-pregnanediol, estrone, and estradiol with this method are representative of both 24-h urine …