Synthesis, characterisation and structure determination of 3-[(1Z)-{2-[bis ({[(2-methylphenyl) methyl] sulfanyl}) methylidene] hydrazin-1-ylidene} methyl] benzene-1, 2 …
A light-yellow crystalline product (1), which was isolated after one week from the filtrate of
the reaction between S-2-methylbenzyldithiocarbazate and 2, 3-dihydroxybenzaldehyde,
was characterised by single crystal X-ray diffraction, FTIR and NMR spectroscopic analyses.
The experimental molecular structure of 1 has been established by X-ray crystallography
and showed, to a first approximation, a planar C 2 N 2 S 2+ dihydroxyphenyl region that has
an almost orthogonal relationship to the rings of the pendant S-bound benzyl groups. This …
the reaction between S-2-methylbenzyldithiocarbazate and 2, 3-dihydroxybenzaldehyde,
was characterised by single crystal X-ray diffraction, FTIR and NMR spectroscopic analyses.
The experimental molecular structure of 1 has been established by X-ray crystallography
and showed, to a first approximation, a planar C 2 N 2 S 2+ dihydroxyphenyl region that has
an almost orthogonal relationship to the rings of the pendant S-bound benzyl groups. This …
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