Synthesis, characterization and antifungal studies of arylspiroborates derived from 4-nitrocatechol

JA Mosseler, JA Melanson, EG Bowes, GM Lee… - Journal of Molecular …, 2011 - Elsevier
A family of arylspiroborates has been prepared by the addition of 4-nitrocatechol, boric acid
and either an alkali metal hydroxide or an ammonium hydroxide. All compounds were
characterized fully using multinuclear NMR spectroscopy, FT-IR spectroscopy and by
elemental analyses. A single crystal X-ray diffraction was carried out on
triethylmethylammonium 4-nitro [1, 2-benzenediolato (2-)-O, O′] borate (5). All new
compounds were tested for potential fungicidal activity.
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