Quantitative analysis of amino and organic acids by methyl chloroformate derivatization and GC-MS/MS analysis
HFN Kvitvang, KA Kristiansen, SK Lien… - Mass Spectrometry in …, 2014 - Springer
… Alkyl chloroformates are known for their ability to produce … reagents for gas chromatographic
(GC) separation of amino- and … Here, we describe a methyl chloroformate (MCF) GC-MS/MS …
(GC) separation of amino- and … Here, we describe a methyl chloroformate (MCF) GC-MS/MS …
Chloroformates in gas chromatography as general purpose derivatizing agents
P Hušek - Journal of Chromatography B: Biomedical Sciences …, 1998 - Elsevier
… chloroformate-mediated ester formation in organic chemistry, … of applications of
chloroformate-mediated derivatization in … treated with hexyl chloroformate and analyzed by …
chloroformate-mediated derivatization in … treated with hexyl chloroformate and analyzed by …
Application of ethyl chloroformate derivatization for gas chromatography–mass spectrometry based metabonomic profiling
… To our knowledge, a GC–MS method with ECF derivatization … The new GC–MS procedure
with ECF derivatization has … compounds belonging to different chemical classes (amino acids, …
with ECF derivatization has … compounds belonging to different chemical classes (amino acids, …
GC-MS with ethyl chloroformate derivatization for comprehensive analysis of metabolites in serum and its application to human uremia
… is an indispensable step in the GC-MS analysis of compounds with … GC-MS assay because
chloroform has a lower volatility than n-hexane and exhibits a better separation in the GC-MS …
chloroform has a lower volatility than n-hexane and exhibits a better separation in the GC-MS …
Alkyl chloroformates in sample derivatization strategies for GC analysis. Review on a decade use of the reagents as esterifying agents
P Husek, P Simek - Current Pharmaceutical Analysis, 2006 - ingentaconnect.com
… Simultaneous determination of 13 FAs, 6 dicarboxylic acids and 13 AAs as IBC-IBE in a
single run by GC-positive ion chemical ionization (PICI) MS using isobutane as reagent gas was …
single run by GC-positive ion chemical ionization (PICI) MS using isobutane as reagent gas was …
A sensitive method for the quantification of short-chain fatty acids by benzyl chloroformate derivatization combined with GC-MS
M Li, R Zhu, X Song, Z Wang, H Weng, J Liang - Analyst, 2020 - pubs.rsc.org
… Propyl chloroformate or isobutyl chloroformate is more widely … Herein a fast and accurate
chemical derivatization-GC-MS … benzyl chloroformate (BCF) and benzyl alcohol for chemical …
chemical derivatization-GC-MS … benzyl chloroformate (BCF) and benzyl alcohol for chemical …
Metabolite analysis of human fecal water by gas chromatography/mass spectrometry with ethyl chloroformate derivatization
X Gao, E Pujos-Guillot, JF Martin, P Galan, C Juste… - Analytical …, 2009 - Elsevier
… Recent work indicates that the revised ethyl chloroformate (ECF… the GC/MS analysis method
coupled with chloroformate … affect the pH value and chemical composition of human fecal …
coupled with chloroformate … affect the pH value and chemical composition of human fecal …
Characterization of N‐methylated amino acids by GC‐MS after ethyl chloroformate derivatization
BS Reddy, VN Chary, P Pavankumar… - Journal of Mass …, 2016 - Wiley Online Library
… applied ethyl chloroformate (ECF) as the derivatization reagent for the GC-MS analysis of
monomethyl and dimethyl amino acids. The present study highlights a simple GC-MS method …
monomethyl and dimethyl amino acids. The present study highlights a simple GC-MS method …
… of synthetic opioids using chloroformate chemistry: Retrospective detection of fentanyl and acetylfentanyl in urine and plasma samples by EI-GC-MS and HR-LC-MS
CA Valdez, RN Leif, TH Corzett, ML Dreyer - Plos one, 2022 - journals.plos.org
… that can be detected by GC-MS. Intrigued by the challenges posed by fentanyl’s chemical
inertness, we explored the use of chloroformate chemistry to investigate its potential for …
inertness, we explored the use of chloroformate chemistry to investigate its potential for …
Analytical platform for metabolome analysis of microbial cells using methyl chloroformate derivatization followed by gas chromatography–mass spectrometry
KF Smart, RBM Aggio, JR Van Houtte… - Nature protocols, 2010 - nature.com
… GC-MS). The protocol is subdivided into sampling, sample preparation, chemical derivatization
of metabolites, GC-MS … a fast chemical derivatization reaction using methyl chloroformate. …
of metabolites, GC-MS … a fast chemical derivatization reaction using methyl chloroformate. …
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