Strategies to avoid false negative findings in residue analysis using liquid chromatography coupled to time‐of‐flight mass spectrometry

A Kaufmann, P Butcher - … Devoted to the Rapid Dissemination of …, 2006 - Wiley Online Library
Liquid chromatography coupled to orthogonal acceleration time-of-flight mass spectrometry
(LC/TOF) provides an attractive alternative to liquid chromatography … ion chromatogram

Method validation for the analysis of 169 pesticides in soya grain, without clean up, by liquid chromatography–tandem mass spectrometry using positive and negative …

IR Pizzutti, A de Kok, R Zanella, MB Adaime… - … of Chromatography A, 2007 - Elsevier
… In total, 155 pesticides were analysed by LC–MS/MS in the ESI positive mode and 14
pesticides in the ESI negative mode, each mode in one single chromatographic run. …

Factors affecting separation and detection of bile acids by liquid chromatography coupled with mass spectrometry in negative mode

S Yin, M Su, G Xie, X Li, R Wei, C Liu, K Lan… - Analytical and …, 2017 - Springer
… work developed three chromatographic gradient methods to … detection of them by liquid
chromatography coupled with mass … effects of the elution pH value on the retention behaviors of …

Rapid determination of chloramphenicol and its glucuronide in food products by liquid chromatography–electrospray negative ionization tandem mass spectrometry

MJ Bogusz, H Hassan, E Al-Enazi, Z Ibrahim… - … of chromatography B, 2004 - Elsevier
chromatography–mass spectrometry. The use of liquid chromatographynegative ionization
electrospray tandem mass spectrometry (LC–ESI–MS–MS) was proven as most selective …

Adulteration identification of commercial honey with the C-4 sugar content of negative values by an elemental analyzer and liquid chromatography coupled to isotope …

H Dong, D Luo, Y Xian, H Luo, X Guo… - Journal of agricultural …, 2016 - ACS Publications
… a value of the C-4 sugar content of ≤7%. In addition, the method reports negative values
calculated with negative values (C-4 sugar content of some honey samples was even more …

… determination of a carboxylic acid compound in human plasma by negative ion electrospray high performance liquid chromatography tandem mass spectrometry

M Jemal, Z Ouyang, DS Teitz - Rapid Communications in Mass …, 1998 - Wiley Online Library
liquid chromatography mobile phase, especially formic acid and ammonium formate, on the
negative … Although the best negative ion electrospray response was obtained with a water/…

… of high-performance liquid chromatography mobile phase components on sensitivity in negative atmospheric pressure chemical ionization liquid chromatography …

WH Schaefercor, F Dixon - Journal of the American Society for Mass …, 1996 - Springer
… One area that has benefited dramatically from the advent of liquid chromatography-atmospheric
pressure ionization-mass spectrometry (LC-API-MS) methodologies is bioanalytical …

The use of high‐flow high performance liquid chromatography coupled with positive and negative ion electrospray tandem mass spectrometry for quantitative …

M Jemal, DB Whigan - Rapid Communications in Mass …, 1998 - Wiley Online Library
… and validated utilizing high flow high performance liquid chromatography (HPLC) for on-line …
, 5 mm) to achieve the required chromatographic separation between the two isomers. For …

Tutorial review on validation of liquid chromatography–mass spectrometry methods: Part I

A Kruve, R Rebane, K Kipper, ML Oldekop, H Evard… - Analytica chimica …, 2015 - Elsevier
… state of the art of method validation in liquid chromatography mass spectrometry (LC–MS) and
… This is necessary because in case of very large intercept values negative apparent values

Fragmentation of toxicologically relevant drugs in negative‐ion liquid chromatography–tandem mass spectrometry

WMA Niessen - Mass spectrometry reviews, 2012 - Wiley Online Library
… The starting point of this study was a set of negative-ion MS–MS mass spectra of
toxicologically relevant compounds collected from three libraries, which in most cases contained …