Rapid analysis of volatile fatty acids in feces by headspace gas chromatography tandem mass spectrometry

Z Jiang, Y Wang, R Chen, Y Zhu… - Chinese Journal of …, 2014 - pesquisa.bvsalud.org
ABSTRACT A rapid headspace gas chromatography tandem mass spectrometric (HS-
GC/MS) method was established for the analysis of volatile fatty acids (VFAs) in the feces …

Rapid analysis of short-chain fatty acid in cerebrospinal fluid-plasma-feces from Beagles by headspace gas chromatography-tandem mass spectrometry

Z JIANG, X LIU, Y WANG, L ZHANG… - Chinese Journal of …, 2015 - ingentaconnect.com
Objective: To study the relationship of short-chain fatty acid (SCFA) in cerebrospinal fluids
and SCFA in plasma and feces from Beagles in physiological state. Methods: Headspace …

Analysis of short-chain fatty acids in fecal samples by headspace-gas chromatography

C Zhang, P Tang, H Xu, Y Weng, Q Tang, H Zhao - Chromatographia, 2018 - Springer
The level of short-chain fatty acids (SCFAs) is related to health benefits. In this study, a static
headspace (HS) gas chromatography method was developed and validated for analyzing …

Analysis of alkaline and neutral volatile metabolites in feces by gas chromatography-tandem mass spectrometry

WU Dan, Y Jun-Jun, Y Fan, BY ZHANG, DU Jie… - Chinese Journal of …, 2017 - Elsevier
A rapid gas chromatography-tandem mass spectrometric (GC-MS) method was developed
for the analysis of alkaline and neutral volatile metabolites of feces from human and rats …

Alternative method for gas chromatography‐mass spectrometry analysis of short‐chain fatty acids in faecal samples

R García‐Villalba, JA Giménez‐Bastida… - Journal of separation …, 2012 - Wiley Online Library
Short‐chain fatty acids are the major end products of bacterial metabolism in the large
bowel. They derive mostly from the bacterial breakdown of carbohydrates and are known to …

Determination of six short‐chain fatty acids in rat feces using headspace solid‐phase dynamic extraction coupled with GC‐MS

L Xing, Q Zhang, J Liu, N Yu… - Journal of Separation …, 2024 - Wiley Online Library
Short‐chain fatty acids (SCFAs) are organic acids with carbon atoms less than six, released
through fermentation products by intestinal microbiome, having multiple physiological …

Optimizing secondary electrospray ionization high-resolution mass spectrometry (SESI-HRMS) for the analysis of volatile fatty acids from gut microbiome

JHJ Lee, J Zhu - Metabolites, 2020 - mdpi.com
Gut microbiota plays essential roles in maintaining gut homeostasis. The composition of gut
microbes and their metabolites are altered in response to diet and remedial agents such as …

Direct Derivatization vs Aqueous Extraction Methods of Fecal Free Fatty Acids for GC–MS Analysis

B Amer, C Nebel, HC Bertram, G Mortensen… - Lipids, 2015 - Springer
A comprehensive and accurate determination of free fatty acids (FFA) is required for fecal
metabolomic investigations. The present study compares three aqueous extraction methods …

Gas chromatographic retention time rule and mass spectrometric fragmentation rule of fatty acids and Its application in food

HQ Wu, XL Huang, XS Lin, F Huang, ZX Zhu… - Chinese Journal of …, 2007 - Elsevier
The fat in food samples was extracted using Soxhlet technique, and in-vial derivatized to
their corresponding methyl ester and subsequently analyzed by GC/MS. Sufficient …

An Improved Validated Method for the Determination of Short-Chain Fatty Acids in Human Fecal Samples by Gas Chromatography with Flame Ionization Detection …

M Smith, L Polite, A Christy, I Edirisinghe… - Metabolites, 2023 - mdpi.com
Short-chain fatty acids (SCFAs) are metabolites produced by the gut microbiota through the
fermentation of non-digestible carbohydrates. Recent studies suggest that the gut microbiota …