Effect of extraction methodologies and solvent selection upon cynaropicrin extraction from Cynara cardunculus leaves

T Bras, LA Neves, JG Crespo, MF Duarte - Separation and Purification …, 2020 - Elsevier
Conventional extraction technologies to recover sesquiterpene lactones, relay on long
extraction periods, with high temperatures, and use of organic solvents, often leading to …

Deep Eutectic Solvents as Efficient Media for the Extraction and Recovery of Cynaropicrin from Cynara cardunculus L. Leaves

ELP De Faria, RS Do Carmo, AFM Cláudio… - International journal of …, 2017 - mdpi.com
In recent years a high demand for natural ingredients with nutraceutical properties has been
witnessed, for which the development of more environmentally-friendly and cost-efficient …

Ultrasound assisted extraction of cynaropicrin from Cynara cardunculus leaves: Optimization using the response surface methodology and the effect of pulse mode

T Brás, AFC Paulino, LA Neves, JG Crespo… - Industrial crops and …, 2020 - Elsevier
In this study, conditions for ultrasound assisted extraction (UAE) of cynaropicrin from Cynara
cardunculus leaves by assessing the effect of pulsed mode and different duty cycles were …

Ionic Liquid‐Assisted Extraction and Isolation of Cynaropicrin and Cnicin from Artichoke and Blessed thistle

H Mizuno, T Usuki - ChemistrySelect, 2018 - Wiley Online Library
The sesquiterpene lactones cynaropicrin and cnicin are isolated from artichoke (Cynara
scolymus) and blessed thistle (Cnicus benedictus), respectively. These natural products …

Impact of extraction parameters and concentration by nanofiltration on the recovery of phenolic compounds from Cynara cardunculus var. altilis: Assessment of …

T Bras, O Guerreiro, MF Duarte, LA Neves - Industrial Crops and Products, 2015 - Elsevier
Cynara cardunculus var. altilis has been reported to be an excellent source of phenolic
compounds. Being extraction methodology a crucial step for final extract properties, batch …

Extraction and recovery processes for cynaropicrin from Cynara cardunculus L. using aqueous solutions of surface-active ionic liquids

ELP de Faria, MV Gomes, AFM Cláudio, CSR Freire… - Biophysical …, 2018 - Springer
Due to the wide range of relevant biological activities and high commercial value of
cynaropicrin, and aiming at developing cost-effective processes, aqueous solutions of ionic …

Lipophilic extracts of Cynara cardunculus L. var. altilis (DC): A source of valuable bioactive terpenic compounds

PAB Ramos, AR Guerra, O Guerreiro… - Journal of agricultural …, 2013 - ACS Publications
Lipophilic extracts of Cynara cardunculus L. var. altilis (DC) from the south of Portugal (Baixo
Alentejo) were studied by gas chromatography–mass spectrometry. One sesquiterpene …

Application of Box–Behnken design for ultrasound‐assisted extraction and recycling preparative HPLC for isolation of anthraquinones from Cassia singueana

S Jibril, N Basar, HM Sirat, RA Wahab… - Phytochemical …, 2019 - Wiley Online Library
Abstract Introduction Cassia singueana Del.(Fabaceae) is a rare medicinal plant used in the
traditional medicine preparations to treat various ailments. The root of C. singueana is a rich …

Quantification of cynaropicrin in artichoke leaf extracts by 1H NMR spectroscopy

V Pieri, H Stuppner - Planta medica, 2011 - thieme-connect.com
The quantification of cynaropicrin in artichoke leaf extracts (ALE) by means of quantitative 1
H NMR was performed. The method relies on solid phase extraction for sample preparation …

Green techniques in comparison to conventional ones in the extraction of Amaryllidaceae alkaloids: Best solvents selection and parameters optimization

SS Takla, E Shawky, HM Hammoda… - … of Chromatography A, 2018 - Elsevier
An undisputed trend in sample preparation at present is to meet the requirements of green
chemistry especially in the field of natural products. Green technology continuously pursues …