The robustness of the refocused INADEQUATE MAS NMR pulse sequence for probing
through-bond connectivities has been demonstrated in a large range of solid-state …

Gramicidin-A, a linear pentadecapeptide (with four tryptophans) forming simplest ion
channels in lipids, is studied as a cesium-complex in an organic solvent and as an SDS …

Recent multiple-quantum MAS NMR experiments have shown that a change in the rotor
phase (and, hence, in the Hamiltonian) between the excitation and reconversion periods …

The NMR spectra of powdered or otherwise non-oriented solids are often poorly resolved
owing to the influence of a variety of anisotropic line-broadening mechanisms. The first …

Nuclear magnetic resonance (NMR) spectroscopy is a powerful technique for analyzing
chemical and biological systems. However, in complex solutions with similar molecular …

A new pulse sequence for high-resolution solid-state heteronuclear double-quantum MAS
NMR spectroscopy of dipolar-coupled spin-1 2 nuclei is introduced. It is based on the five …

Spin counting in solid-state NMR spectroscopy requires the use of a reference standard to
calibrate the magnetization detected from the unknown material. Quantitation is performed …

The combination of new magnet and probe technology with increasingly sophisticated pulse
sequences has resulted in an increase in the number of applications of solid-state nuclear …

A new approach for high-resolution solid-state heteronuclear multiple-quantum MAS NMR
spectroscopy of dipolar-coupled spin-1 2 nuclei is introduced. The method is a …

Possibilities and limitations of iterative lineshape fitting procedures of MAS NMR spectra of
isolated homonuclear spin pairs, aiming at determination of magnitudes and orientations of …