Determination of serum uric acid using high-performance liquid chromatography (HPLC)/isotope dilution mass spectrometry (ID-MS) as a candidate reference method

X Dai, X Fang, C Zhang, R Xu, B Xu - Journal of Chromatography B, 2007 - Elsevier
… A group of work standard solutions of natural uric acid was prepared by diluting the stock …
uric acid was prepared by dilution of the stock labeled uric acid solution. Then this labeled …

Determination of serum uric acid by isotope dilution mass spectrometry as a new candidate definitive method

P Ellerbe, A Cohen, MJ Welch, EV White - Analytical chemistry, 1990 - ACS Publications
… To test for complete equilibration of labeled uric acid and endogenous uric acid in serum,
we spiked a serum sample with a solution of labeled uric acid. After mixing, the solution was …

Determination of uric acid in human serum by isotope dilution-mass spectrometry. Definitive methods in clinical chemistry, III

L Siekmann - 1985 - degruyter.com
… 5 μg uric acid (the approximate concentration of uric acid is estimated in a preliminary experiment)
are sampled and diluted … Twenty μΐ of the [l,3-15NJuric acid solution are added to the …

… method for the determination of uric acid in serum based on high performance liquid chromatography, compared with an isotope dilution-gas chromatography-mass …

R Kock, B Delvoux, U Tillmanns, H Greiling - 1989 - degruyter.com
… for the determination of uric acid. Data obtained … dilution-gas chromatography-mass
spectrometric method (ID-GC-MS), using [l,3-15N2]uric acid äs internal Standard and selected mass

… uric acid-related compounds in urine using a “dilute-and-shoot” technique coupling ultra-high-performance liquid chromatography and high-resolution Orbitrap mass …

A Rodriguez, RM Gomila, G Martorell… - … of Chromatography B, 2017 - Elsevier
uric acid crystallization with potential application in the treatment and prevention of uric acid
… prepared in 0.1% formic acid and serially diluted in 0.1% formic acid solution to prepare the …

Measurement of serum uric acid by isotope dilution liquid chromatography tandem mass spectrometry: Modification of a candidate reference measurement method …

J Yan, H Lin, Y Xu, L Yu, S Chen, Q Zhang… - … Journal of Mass …, 2022 - Elsevier
… , and regular monitoring of uric acid concentration is essential … dilution coupled with liquid
chromatography-tandem mass spectrometry (ID-LC-MS/MS) method for human serum uric acid

[PDF][PDF] Measurement of serum uric acid by liquid chromatography.

LA Pachla, PT Kissinger - Clinical chemistry, 1979 - researchgate.net
… WI 53233)2 and mix until the uric acid is dissolved … the uric acid solution to a 500-mL
volumetric flask and dilute to … Allow the solution to cool to room temperature, mix, dilute to volume, …

Determination of uric acid in urine, saliva and calcium oxalate renal calculi by high-performance liquid chromatography/mass spectrometry

J Perelló, P Sanchis, F Grases - Journal of Chromatography B, 2005 - Elsevier
… of uric acid, in various biological matrices, based on high-performance liquid chromatography
and mass … amounts of uric acid in the core of some selected calcium oxalate renal calculi. …

The stability of uric acid in ammonium hydroxide.

P Ellerbe, A Cohen, MJ Welch, E White - Clinical chemistry, 1988 - academic.oup.com
… stability of uric acid in dilute aqueous ammonium hydroxide solution by mass spectrometry.
… mole ratio of ammonium hydroxide to uric acid of 3.4, uric acid is not detectably decomposed. …

Recent progress on uric acid detection: a review

Q Wang, X Wen, J Kong - Critical reviews in analytical chemistry, 2020 - Taylor & Francis
… ), electrochemical (voltammetry, electrochemiluminescence, surface plasmon resonance),
chromatography (liquid and gas phase), capillary electrophoresis and isotope dilution mass