. alpha.-Azidonation of Amides, Carbamates, and Ureas with the Iodosylbenzene/Trimethylsilyl Azide Reagent Combination: N-Acyliminium Ion Precursors
P Magnus, C Hulme, W Weber - Journal of the American Chemical …, 1994 - ACS Publications
P Magnus, C Hulme, W Weber
Journal of the American Chemical Society, 1994•ACS Publications(3) If this solution is warmed to 0 C, it cleanly decomposes to iodobenzene, nitrogen, and
hexamethyldisiloxane. For the decomposition of TMSN3/PhIO to dinitrogen, iodobenzene,
and hexamethyldisiloxane, see: Zefirov, NS; Safronov, SO; Kaznacheev, AA; Zhdankin, VV
Zh. Org. Khim. 1989, 25, 1807; 1990, 25, 1633.
hexamethyldisiloxane. For the decomposition of TMSN3/PhIO to dinitrogen, iodobenzene,
and hexamethyldisiloxane, see: Zefirov, NS; Safronov, SO; Kaznacheev, AA; Zhdankin, VV
Zh. Org. Khim. 1989, 25, 1807; 1990, 25, 1633.
(3) If this solution is warmed to 0 C, it cleanly decomposes to iodobenzene, nitrogen, and hexamethyldisiloxane. For the decomposition of TMSN3/PhIO to dinitrogen, iodobenzene, and hexamethyldisiloxane, see: Zefirov, N. S.; Safronov, S. O.; Kaznacheev, AA; Zhdankin, VV Zh. Org. Khim. 1989, 25, 1807; 1990, 25, 1633.
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