In situ U–Pb SIMS (IN-SIMS) micro-baddeleyite dating of mafic rocks: method with examples

KR Chamberlain, AK Schmitt, SM Swapp… - Precambrian …, 2010 - Elsevier
KR Chamberlain, AK Schmitt, SM Swapp, TM Harrison, N Swoboda-Colberg, W Bleeker
Precambrian Research, 2010Elsevier
An in situ U–Pb SIMS (IN-SIMS) method to date micro-baddeleyite crystals as small as 3μm
is presented with results from three samples that span a variety of ages and geologic
settings. The method complements ID-TIMS geochronology by extending the range of
dateable crystals to sizes smaller than can be recovered by physical separation. X-ray
mapping and BSE imaging are used to locate target grains in thin section, followed by SIMS
analysis on a CAMECA ims 1270, using the field aperture in the transfer column to screen …
An in situ U–Pb SIMS (IN-SIMS) method to date micro-baddeleyite crystals as small as 3μm is presented with results from three samples that span a variety of ages and geologic settings. The method complements ID-TIMS geochronology by extending the range of dateable crystals to sizes smaller than can be recovered by physical separation. X-ray mapping and BSE imaging are used to locate target grains in thin section, followed by SIMS analysis on a CAMECA ims 1270, using the field aperture in the transfer column to screen out ions from host phases. Internal age precisions for the method are anticipated to range from 0.1% for Precambrian rocks to 3–7% for Phanerozoic rocks. Results establish a 2689±5Ma age for mafic dikes in the Wyoming craton, USA, a 1540±30Ma age for a subaerial lava flow from the Thelon Basin of northern Canada, and a 457±34Ma age for mafic dikes in the platform sequence of southeastern Siberia. The method is ideal for relatively non-destructive dating of small samples such as extraterrestrial rocks and precious terrestrial samples.
Elsevier
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