Synthesis and Characterization of Core-Shell Nanowires

JH Lee, JH Wu, JS Lee, KS Jeon… - IEEE Transactions …, 2008 - ieeexplore.ieee.org
JH Lee, JH Wu, JS Lee, KS Jeon, HR Kim, JH Lee, YD Suh, YK Kim
IEEE Transactions on Magnetics, 2008ieeexplore.ieee.org
We report the synthesis and characterization of Fe-FeO x core-shell nanowires by thermal
conversion of the Fe nanowires from pulse electrodeposition in anodized aluminum oxide
(AAO) nanotemplates under various conditions. Well-defined core-shell nanostructure of the
Fe-FeO x nanowires was confirmed by TEM and corresponding elemental line scanning and
point scanning. The type of the iron oxide in the shell was identified using nano-Raman
spectroscopy, which exposes magnetite to be the major constituent. The magnetic …
We report the synthesis and characterization of Fe-FeO x core-shell nanowires by thermal conversion of the Fe nanowires from pulse electrodeposition in anodized aluminum oxide (AAO) nanotemplates under various conditions. Well-defined core-shell nanostructure of the Fe-FeO x nanowires was confirmed by TEM and corresponding elemental line scanning and point scanning. The type of the iron oxide in the shell was identified using nano-Raman spectroscopy, which exposes magnetite to be the major constituent. The magnetic measurements demonstrate that the nanowires are robustly soft magnetic, with the magnetization tunable by heat treatment parameters and a weak magnetic easy direction parallel to the nanowire axis.
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