Synthesis of the biocompatible and highly stable MIL-127 (Fe): from large scale synthesis to particle size control
H Chevreau, A Permyakova, F Nouar, P Fabry… - …, 2016 - pubs.rsc.org
H Chevreau, A Permyakova, F Nouar, P Fabry, C Livage, F Ragon, A Garcia-Marquez…
CrystEngComm, 2016•pubs.rsc.org… The synthesis of this solid was optimized at the multigram scale avoiding the use of
hazardous Fe(ClO 4 ) 3 , previously used as an iron precursor (this solid will be further
denoted as MIL-127(DMF)). Then, to develop an environmentally friendly synthetic route,
compatible with biomedical applications, among others, MIL-127 was successfully prepared
using propan-2-ol as solvent (denoted as MIL-127(Prop)). A time-resolved in situ EDXRD
study of the … The biocompatible and highly stable iron(III) tetracarboxylate MIL-127(Fe) …
hazardous Fe(ClO 4 ) 3 , previously used as an iron precursor (this solid will be further
denoted as MIL-127(DMF)). Then, to develop an environmentally friendly synthetic route,
compatible with biomedical applications, among others, MIL-127 was successfully prepared
using propan-2-ol as solvent (denoted as MIL-127(Prop)). A time-resolved in situ EDXRD
study of the … The biocompatible and highly stable iron(III) tetracarboxylate MIL-127(Fe) …
Controlled-sized crystals, from the nano to the microscale, of the biocompatible and highly stable porous iron(III) 3,3,′5,5′-azobenzenetetracarboxylate MIL-127(Fe) MOF have been successfully prepared with very high space-time-yields using different synthetic routes.
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