Advances in sample preparation in electromigration, chromatographic and mass spectrometric separation methods

M Gilar, ESP Bouvier, BJ Compton - Journal of Chromatography A, 2001 - Elsevier
The quality of sample preparation is a key factor in determining the success of analysis.
While analysis of pharmaceutically important compounds in biological matrixes has driven …

Particle-loaded membranes for sample concentration and/or clean-up in bioanalysis

H Lingeman, SJF Hoekstra-Oussoren - Journal of Chromatography B …, 1997 - Elsevier
Solid-phase extraction nowadays is a major sample preparation tool. The latest
development in this area is the introduction of particle-loaded membranes (membrane …

Solvation parameter model for the prediction of breakthrough volumes in solid-phase extraction with particle-loaded membranes

ML Larrivee, CF Poole - Analytical Chemistry, 1994 - ACS Publications
The experimental factors which establish the breakthrough volume in solid-phase extraction
áre interpreted using a theoretical modelproposed by Lovkvist and Jonsson. For …

Optimized high-performance liquid chromatographic method for determination of lamotrigine in serum with concomitant determination of phenytoin, carbamazepine …

GL Lensmeyer, BE Gidal, DA Wiebe - Therapeutic drug monitoring, 1997 - journals.lww.com
Abstract Lamotrigine (LG), phenytoin (PY), carbamazepine (CM), and carbamazepine
epoxide (CE) are measured with an optimized procedure that uses thin sorbent extraction …

Use of metal chelate affinity chromatography and membrane-based ion-exchange as clean-up procedure for trace residue analysis of tetracyclines in animal tissues …

SM Croubels, KEI Vanoosthuyze… - … of Chromatography B …, 1997 - Elsevier
A new and efficient procedure for the clean-up of tetracycline residues in animal tissues and
egg prior to reversed-phase high-performance liquid chromatography is described. The …

Optimized method for determination of gabapentin in serum by high-performance liquid chromatography

GL Lensmeyer, T Kempf, BE Gidal… - Therapeutic drug …, 1995 - journals.lww.com
The anticonvulsant drug gabapentin and its heptaneacetic acid analog—used here as an
internal standard—are isolated from serum (pH 9) with an octyldecyl (C-18) solid-phase …

[图书][B] Postmortem toxicology of abused drugs

F MD, SB Karch - 2007 - api.taylorfrancis.com
Extracted from the Drug Abuse Handbook, 2nd edition, to give you just the information you
need at an affordable price. Postmortem Toxicology of Abused Drugs considers the role of …

Investigation of the kinetic properties of particle-loaded membranes for solid-phase extraction by forced flow planar chromatography

WPN Fernando, ML Larrivee, CF Poole - Analytical Chemistry, 1993 - ACS Publications
Planar chromatography with forced-flow development Is used to characterize the kineticand
some thermodynamic properties of octadecylsllanlzed silica particle-loaded membranes …

Application of Empore disk extraction for trace analysis of spinosad and metabolites in leafy vegetables, peppers, and tomatoes by high-performance liquid …

LT Yeh, DA Schwedler, GE Schelle… - Journal of Agricultural …, 1997 - ACS Publications
Residue methods were developed for the quantitation of spinosad and metabolites in leafy
vegetables, peppers, and tomatoes. The compounds were extracted with a solution of …

Identification of the procedural steps that affect recovery of semi-volatile compounds by solid-phase extraction using cartridge and particle-loaded membrane (disk) …

ML Mayer, CF Poole - Analytica chimica acta, 1994 - Elsevier
The experimental conditions are optimized for the recovery of a test mixture of neutral semi-
volatile analytes on a cartridge and particle-loaded membrane (disk) device used for solid …