Optimization and validation of a head space solid-phase microextraction-arrow gas chromatography-mass spectrometry method using central composite design for …

X Zhang, C Wang, L Wang, S Chen, Y Xu - Journal of Chromatography A, 2020 - Elsevier
A headspace solid-phase microextraction Arrow (HS-SPME Arrow) method coupled with gas
chromatography-mass spectrometry (GC–MS) was developed for the quantitation of a large …

Aroma dilution method using GC injector split ratio for volatile compounds extracted by headspace solid phase microextraction

TH Kim, SM Lee, YS Kim, KH Kim, S Oh, HJ Lee - Food Chemistry, 2003 - Elsevier
Dilution methods are widely used for the screening of aroma-active compounds in gas
chromatography-olfactometry (GC-O). An aroma dilution method for the samples extracted …

HS-SPME and SDE combined with GC–MS and GC-O for characterization of flavor compounds in Zhizhonghe Wujiapi medicinal liquor

L Ma, W Gao, F Chen, Q Meng - Food Research International, 2020 - Elsevier
Volatile compounds in Chinese medicinal liquor, Zhizhonghe Wujiapi (WJP liquor), were
extracted by headspace-solid-phase microextraction (HS-SPME) and simultaneous …

Preparation of novel solid-phase microextraction fibers by sol–gel technology for headspace solid-phase microextraction-gas chromatographic analysis of aroma …

M Liu, Z Zeng, B Xiong - Journal of Chromatography A, 2005 - Elsevier
3-(Trimethoxysilyl) propyl methacrylate (TMSPMA) was first used as precursor as well as
selective stationary phase to prepare the sol–gel-derived TMSPMA-hydroxyl-terminated …

Comparison of headspace–SPME and SPME-Arrow–GC–MS methods for the determination of volatile compounds in Korean salt–fermented fish sauce

NE Song, JY Lee, YY Lee, JD Park… - Applied Biological …, 2019 - Springer
A new solid phase microextraction (SPME)-Arrow method was evaluated for the analysis of
volatile compounds in kanari-aekjeot, a Korean traditional salt–fermented sand lance sauce …

Optimisation of a simple and reliable method based on headspace solid-phase microextraction for the determination of volatile phenols in beer

C Pizarro, N Pérez-del-Notario… - … of Chromatography A, 2010 - Elsevier
A simple, accurate and sensitive method based on headspace solid-phase microextraction
(HS-SPME) coupled to gas chromatography–tandem mass spectrometry (GC–MS/MS) was …

Solid-phase microextraction for headspace analysis of key volatile compounds in orange beverage emulsion

H Mirhosseini, Y Salmah, SAH Nazimah, CP Tan - Food Chemistry, 2007 - Elsevier
Headspace solid-phase microextraction (HS-SPME) gas chromatography was used to
analyze target flavor compounds in orange beverage emulsion. The effects of SPME fiber …

Optimization of headspace solid phase microextraction (HS-SPME) for gas chromatography mass spectrometry (GC–MS) analysis of aroma compounds in cooked …

QL Ma, N Hamid, AED Bekhit, J Robertson… - Microchemical Journal, 2013 - Elsevier
The optimization of the main experimental variables, such as equilibrium time (5–10min),
extraction time (10–50min) and extraction temperature (20–60° C) of a headspace solid …

HS‐SPME/GC‐MS and chemometrics for volatile composition of Chinese traditional aromatic vinegar in the Zhenjiang region

YJ Yu, ZM Lu, NH Yu, W Xu, GQ Li… - Journal of the Institute …, 2012 - Wiley Online Library
The main purpose of this study was to determine the volatile composition of Zhenjiang
aromatic vinegar, one of the four famous China‐style cereal vinegars, by using headspace …

Determination of volatile organic acids in oriental tobacco by needle-based derivatization headspace liquid-phase microextraction coupled to gas chromatography …

SH Sun, JP Xie, FW Xie, YL Zong - Journal of chromatography A, 2008 - Elsevier
A method coupling needle-based derivatization headspace liquid-phase microextraction
with gas chromatography–mass spectrometry (HS-LPME/GC–MS) was developed to …