Optimisation of spatially‐encoded diffusion‐ordered NMR spectroscopy for the analysis of mixtures

C Jacquemmoz, R Mishra, L Guduff… - Magnetic …, 2022 - Wiley Online Library
Diffusion‐ordered NMR spectroscopy (DOSY NMR) is a widely used method for the analysis
of mixtures. It can be used to separate the spectra of a mixture's components and to analyse …

Spatially encoded 2D and 3D diffusion-ordered NMR spectroscopy

L Guduff, I Kuprov, C Van Heijenoort… - Chemical …, 2017 - pubs.rsc.org
We show that the acquisition of 3D diffusion-ordered NMR spectroscopy (DOSY)
experiments can be accelerated significantly with the use of spatial encoding (SPEN). The …

Spatially encoded diffusion-ordered NMR spectroscopy of reaction mixtures in organic solvents

G Hamdoun, L Guduff, C van Heijenoort, C Bour… - Analyst, 2018 - pubs.rsc.org
Diffusion-ordered NMR spectroscopy (DOSY) is a powerful method for the analysis of
mixtures. Classic DOSY methods require several minutes of acquisition, and we show here …

Assessment of techniques for DOSY NMR data processing

R Huo, R Wehrens, J Van Duynhoven… - Analytica chimica …, 2003 - Elsevier
Diffusion-ordered spectroscopy (DOSY) NMR is based on a pulse-field gradient spin-echo
NMR experiment, in which components experience diffusion. Consequently, the signal of …

Directly decoupled diffusion‐ordered NMR spectroscopy for the analysis of compound mixtures

S Glanzer, K Zangger - Chemistry–A European Journal, 2014 - Wiley Online Library
For the analysis of compound mixtures by NMR spectroscopy, it is important to assign the
different peaks to the individual constituents. Diffusion‐ordered spectroscopy (DOSY) is …

Acceleration of 3D DOSY NMR by Spatial Encoding of the Chemical Shift

C Jacquemmoz, JN Dumez - ChemPhysChem, 2018 - Wiley Online Library
Diffusion‐ordered NMR spectroscopy (DOSY) is a powerful method for the analysis of
solution mixtures. With 3D DOSY, the 2D NMR spectra of a mixture's components can be …

A homodecoupled diffusion experiment for the analysis of complex mixtures by NMR

JC Cobas, M Martin-Pastor - Journal of Magnetic Resonance, 2004 - Elsevier
Diffusion ordered spectroscopy (DOSY) relies on differences in translation diffusion as a
means to separate components in a solution mixture. However, the analysis of spectra of …

Pulsed-field gradient nuclear magnetic resonance measurements (PFG NMR) for diffusion ordered spectroscopy (DOSY) mapping

G Pagès, V Gilard, R Martino, M Malet-Martino - Analyst, 2017 - pubs.rsc.org
While NMR is the most used analytical method for determining the molecular structure of
isolated chemical entities, small compounds as well as macromolecules, its capability of …

Matrix-assisted diffusion-ordered spectroscopy

R Evans, IJ Day - RSC advances, 2016 - pubs.rsc.org
Diffusion NMR is a potentially routine tool in the analysis of mixtures, from industrial and
synthetic outputs to natural products. However, the technique struggles to resolve species of …

A pure shift and spin echo based approach for high-resolution diffusion-ordered NMR spectroscopy

C Li, H Zhan, J Yan, M Hao, E Lin, Y Huang… - Journal of Magnetic …, 2019 - Elsevier
Diffusion-ordered NMR spectroscopy (DOSY) can be used for separating mixture
components according to their individual diffusion behaviors, thus offering a powerful tool for …