Assessment of the sample handling procedures in a labor-saving method for the analysis of organochlorine compounds in a large number of fish samples

L Berdié, JO Grimalt - Journal of Chromatography A, 1998 - Elsevier
A rapid single step clean-up procedure with sulphuric acid oxidation for lipid removal has
been assessed by a step-by-step recovery approach for its performance in the analysis of …

A comparative evaluation of accelerated solvent extraction and Polytron extraction for quantification of lipids and extractable organochlorine in fish

W Zhuang, B McKague, D Reeve, J Carey - Chemosphere, 2004 - Elsevier
Optimal conditions for extraction methods using an accelerated solvent extractor (ASE) and
a Polytron homogenizer were established for quantification of (crude) lipids and extractable …

Rapid determination of organochlorine pesticides in fish using selective pressurized liquid extraction and gas chromatography–mass spectrometry

M Choi, IS Lee, RH Jung - Food Chemistry, 2016 - Elsevier
A rapid automated extraction and cleanup method using selective pressurized liquid
extraction was developed and validated for 14 organochlorine pesticides in fish. The lipid …

Variability in organochlorine analysis in fish: An interlaboratory study and its implications for environmental monitoring and regulatory standards

AG Miskiewicz, PJ Gibbs - Archives of environmental contamination and …, 1992 - Springer
Samples of muscle, from four types of fish, that had been spiked at 0.25 and 1.0 mg/kg with
hexachlorobenzene (HCB), gamma BHC (lindane), technical chlordane, p, p′-DDT, p, p …

Rapid determination of chlorinated pesticides in fish by freezing-lipid filtration, solid-phase extraction and gas chromatography–mass spectrometry

J Hong, HY Kim, DG Kim, J Seo, KJ Kim - Journal of Chromatography A, 2004 - Elsevier
An analytical method has been developed for measuring 24 chlorinated pesticides in fish
tissue samples. Extraction of chlorinated pesticides was carried out by ultrasonication using …

Determination of low concentrations of organochlorine pesticides and PCBs in fish feed and fish tissues from aquaculture activities by gas chromatography with …

R Serrano, M Barreda, E Pitarch… - Journal of separation …, 2003 - Wiley Online Library
A sensitive and rapid multiresidual method has been developed for the determination of
organochlorine compounds in fish feed and fish tissues. The method is based on automated …

Determination of selected chlorinated priority substances in fish using QuEChERS method with dual dSPE clean-up and gas chromatography

P Tölgyessy, Z Miháliková, M Matulová - Chromatographia, 2016 - Springer
A rapid and simple analytical method for the determination of ten chlorinated priority
substances (hexachloro-1, 3-butadiene, pentachlorobenzene, hexachlorobenzene …

Multiresidue determination of persistent organochlorine and organophosphorus compounds in whale tissues using automated liquid chromatographic clean up and …

R Serrano, FJ López, F Hernández - Journal of Chromatography A, 1999 - Elsevier
A multiresidue method based on normal-phase LC for the sample clean up of whale tissues
extracts prior to GC–MS determination of residues of polychlorinated biphenyls …

Some aspects of the recovery of chlorinated residues (DDT-type compounds and PCB) from fish tissue by using different extraction methods

ML Hattula - Bull. Environ. Contam. Toxicol, 1974 - hero.epa.gov
In this study four solvent systems were studied and used as cold extraction in glass columns
and as hot extraction in Soxhlet apparatus. The four systems included: diethyl ether; diethyl …

Determination of organochlorine compounds in fatty matrices application of rapid off-line normal-phase liquid chromatographic clean-up

GR van der Hoff, AC Van Beuzekom, A Udo… - … of Chromatography A, 1996 - Elsevier
A clean-up method for organochlorine compounds in fatty samples based on normal-phase
liquid chromatography (NPLC) is described. To this end, an existing clean-up procedure …