Hydrothermal Crystal Growth and Structure Determination of Double Hydroxides LiSb(OH)6, BaSn(OH)6, and SrSn(OH)6

H Mizoguchi, NSP Bhuvanesh, YI Kim… - Inorganic …, 2014 - ACS Publications
Colorless single crystals of LiSb (OH) 6, SrSn (OH) 6, and BaSn (OH) 6, which are useful as
precursors for the synthesis of LiSbO3, SrSnO3, and BaSnO3, were synthesized by a low …

Structural study of a series of layered rare-earth hydroxide sulfates

F Geng, R Ma, Y Matsushita, J Liang… - Inorganic …, 2011 - ACS Publications
We report structure analysis of a new family of rare-earth hydroxides Ln2 (OH) 4SO4· 2H2O
(Ln= Pr, Nd, Sm, Eu, Gd, Tb) from synchrotron X-ray and electron diffraction data. Rietveld …

Synthesis and Crystal Growth of Two Novel Layered Structures, NaKLaNbO5 and Na2K2Gd4Nb2O13, in Molten Hydroxide Salts

JH Liao, MC Tsai - Crystal growth & design, 2002 - ACS Publications
NaKLaNbO5 (1) and Na2K2Gd4Nb2O13 (2) were synthesized and crystallized by reacting
La2O3 or Gd2O3 with Nb2O5 in molten NaOH/KOH hydroxide salts at 400 and 450° C …

Hydrothermal synthesis and structural characterization of a novel hydroxo stannate: Sr2Sn (OH) 8

M Wu, X Li, G Shen, J Li, R Xu, DM Proserpio - Journal of Solid State …, 2000 - Elsevier
A new hydroxo stannate (IV), Sr2Sn (OH) 8, has been synthesized by the hydrothermal
method. Single-crystal X-ray diffraction shows that this compound crystallizes in the …

Hydrothermal Synthesis and Crystal Structure of Two New Hydrated Alkaline Earth Metal Borates Sr3B6O11(OH)2 and Ba3B6O11(OH)2

C Heyward, C McMillen, J Kolis - Inorganic Chemistry, 2012 - ACS Publications
Two new hydrated borates Sr3B6O11 (OH) 2 (1) and Ba3B6O11 (OH) 2 (2) were
hydrothermally synthesized. Their structures were determined by single-crystal X-ray …

Controlled Hydrothermal Crystallization of Anhydrous Ln2(OH)4SO4 (Ln=Eu–Lu, Y) as a New Family of Layered Rare Earth Metal Hydroxides

X Wang, MS Molokeev, Q Zhu… - Chemistry–A European …, 2017 - Wiley Online Library
Anhydrous hydroxide sulfates Ln2 (OH) 4SO4 (Ln= Eu–Lu, Y) were hydrothermally
synthesized as a new family of layered rare earth metal hydroxides (LRHs). They crystallize …

Alkaline-Earth Rhodium Hydroxides: Synthesis, Structures, and Thermal Decomposition to Complex Oxides

DS Cook, GJ Clarkson, DM Dawson… - Inorganic …, 2018 - ACS Publications
The rhodium (III) hydrogarnets Ca3Rh2 (OH) 12 and Sr3Rh2 (OH) 12 crystallize as
polycrystalline powders under hydrothermal conditions at 200° C from RhCl3· 3H2O and …

Ln2(OH)4SO4·nH2O (Ln = Pr to Tb; n ∼ 2): A New Family of Layered Rare-Earth Hydroxides Rigidly Pillared by Sulfate Ions

J Liang, R Ma, F Geng, Y Ebina, T Sasaki - Chemistry of Materials, 2010 - ACS Publications
A new family of layered rare-earth hydroxides rigidly pillared by sulfate ions has been
synthesized through homogeneous precipitation of lanthanide sulfate salts driven by …

Crystal structures of the novel hydrated borates Ba2B5O9 (OH), Sr2B5O9 (OH) and Li2Sr8B22O41 (OH) 2

C McMillen, C Heyward, H Giesber, J Kolis - Journal of Solid State …, 2011 - Elsevier
Three novel hydrated borates Ba2B5O9 (OH)(1), Sr2B5O9 (OH)(2) and Li2Sr8B22O41 (OH)
2 (3) have been synthesized hydrothermally and their structures determined. Compounds …

Sr4AlNbO8: A new crystal structure type determined from powder X-ray data

E Lee, ST Hong - Journal of Solid State Chemistry, 2008 - Elsevier
Sr4AlNbO8 was synthesized at 1500° C in air. The crystal structure was initially determined
from powder X-ray diffraction data, and later refined with combined X-ray and neutron …