Controlled microwave heating in modern organic synthesis: highlights from the 2004–2008 literature

CO Kappe, D Dallinger - Molecular diversity, 2009 - Springer
Direct and rapid heating by microwave irradiation in combination with sealed vessel
processing in many cases enables reactions to be carried out in a fraction of the time …

Microwave enhanced synthesis

S Caddick, R Fitzmaurice - Tetrahedron, 2009 - Elsevier
Microwave technology has become very important in synthesis and it is reasonable to assert
that there are now very few areas of synthetic organic chemistry that have not been shown to …

Chemo-/regioselective synthesis of 6-unsubstituted dihydropyrimidinones, 1, 3-thiazines and chromones via novel variants of Biginelli reaction

JP Wan, YJ Pan - Chemical communications, 2009 - pubs.rsc.org
A novel and facile cascade Biginelli-like assembly employing enaminone, aldehyde and
urea/thiourea has been developed, which provides a highly chemo-and regioselective …

New advances in the synthesis of Biginelli 3, 4-dihydropyrimidin-2 (1H)-one derivatives

Z Quan, Z Zhang, Y Da, X Wang - Chinese Journal of Organic …, 2009 - sioc-journal.cn
In 1893, Biginelli reported the first synthesis of 3, 4-dihydropyrimidin-2 (1H)-ones (DHPM) by
a very simple one-pot condensation reaction of an aromatic aldehyde, urea and ethyl …

A Multicomponent Reaction Towards N‐(Cyanomethyl)amides

N Elders, E Ruijter, FJJ de Kanter… - … A European Journal, 2009 - Wiley Online Library
Diversity‐oriented synthesis: The multicomponent reaction of α‐isocyano amides, aldehydes
or ketones, and amines affords N‐(cyanomethyl) amides, presenting the fourth class of …

Fast surface modification by microwave assisted click reactions on silicon substrates

C Haensch, T Erdmenger, MWM Fijten, S Hoeppener… - Langmuir, 2009 - ACS Publications
Microwave irradiation has been used for the chemical modification of functional monolayers
on silicon surfaces. The thermal and chemical stability of these layers was tested under …

Biginelli 3, 4-二氢嘧啶-2-酮衍生物的合成研究新进展

权正军, 张彰, 达玉霞, 王喜存 - 有机化学, 2009 - sioc-journal.cn
摘要1893 年, 意大利化学家Biginelli 首次利用芳香醛, 乙酰乙酸乙酯和尿素三组分“一锅煮法”
合成了3, 4-二氢嘧啶-2 (1H)-酮. 此类化合物具有良好的生物活性和反应活性, 对近几年来有关 …

Synthesis of Boltorn 1, 2, 3‐triazole dendrimers by click chemistry

AR Katritzky, Y Song, R Sakhuja… - Journal of Polymer …, 2009 - Wiley Online Library
Abstract Second‐, third‐, and fourth‐generation hyperbranched aliphatic polyols namely
Boltorn® H20, Boltorn H30, and Boltorn H40 were endcapped with azido and activated …

Microwave-assisted ruthenium-catalyzed reactions

F Nicks, Y Borguet, S Delfosse… - Australian journal of …, 2009 - CSIRO Publishing
Since the first reports on the use of microwave irradiation to accelerate organic chemical
transformations, a plethora of papers has been published in this field. In most examples …

General and green synthesis of C-6 sulfonylmethyl 4-aryl-3, 4-dihydropyrimidinones in water

ZJ Quan, QB Wei, DD Ma, YX Da… - Synthetic …, 2009 - Taylor & Francis
A simple, inexpensive, and green reaction permitting the synthesis of new C-6
arylsulfonylmethyl 4-aryl-3, 4-dihydropyrimidinones in water by S-alkylation of 6 …