Application of microwave-assisted heterogeneous catalysis in sustainable synthesis design
An overview of recent advances, mainly focusing on the past 5–6 years, in microwave-
assisted heterogeneous catalysis is provided. The work includes three major parts;(i) a …
assisted heterogeneous catalysis is provided. The work includes three major parts;(i) a …
My twenty years in microwave chemistry: from kitchen ovens to microwaves that aren't microwaves
CO Kappe - The chemical record, 2019 - Wiley Online Library
Abstract This Personal Account describes the author's involvement in the field of microwave‐
assisted organic synthesis (MAOS) from the late 1990's starting out with kitchen microwave …
assisted organic synthesis (MAOS) from the late 1990's starting out with kitchen microwave …
The microwave‐to‐flow paradigm: translating high‐temperature batch microwave chemistry to scalable continuous‐flow processes
TN Glasnov, CO Kappe - Chemistry–A European Journal, 2011 - Wiley Online Library
The popularity of dedicated microwave reactors in many academic and industrial
laboratories has produced a plethora of synthetic protocols that are based on this enabling …
laboratories has produced a plethora of synthetic protocols that are based on this enabling …
How do the fine chemical, pharmaceutical, and related industries approach green chemistry and sustainability?
WJW Watson - Green Chemistry, 2012 - pubs.rsc.org
Developing manufacturing processes for active pharmaceutical ingredients and
intermediates often involves complex chemistry. All companies now aim to uphold the …
intermediates often involves complex chemistry. All companies now aim to uphold the …
Microwave Flow: A Perspective on Reactor and Microwave Configurations and the Emergence of Tunable Single‐Mode Heating Toward Large‐Scale Applications
JP Barham, E Koyama, Y Norikane… - The Chemical …, 2019 - Wiley Online Library
Microwave heating in chemical reactions was first reported in 1986. There have since been
many reports employing microwave heating in organic chemistry, where microwave heating …
many reports employing microwave heating in organic chemistry, where microwave heating …
Continuous flow synthesis of heterocycles: A recent update on the flow synthesis of indoles
Indole derivatives are among the most useful and interesting heterocycles employed in drug
discovery and medicinal chemistry. In addition, flow chemistry and flow technology are …
discovery and medicinal chemistry. In addition, flow chemistry and flow technology are …
Single-mode microwave reactor used for continuous flow reactions under elevated pressure
M Nishioka, M Miyakawa, Y Daino… - Industrial & …, 2013 - ACS Publications
We present a flow type single-mode microwave (MW) reactor that forms a uniform
electromagnetic field along a tubular reactor (quartz glass, id 1.5 mm× 100 mm) located in …
electromagnetic field along a tubular reactor (quartz glass, id 1.5 mm× 100 mm) located in …
Design and performance validation of a conductively heated sealed-vessel reactor for organic synthesis
D Obermayer, D Znidar, G Glotz, A Stadler… - The Journal of …, 2016 - ACS Publications
A newly designed robust and safe laboratory scale reactor for syntheses under sealed-
vessel conditions at 250° C maximum temperature and 20 bar maximum pressure is …
vessel conditions at 250° C maximum temperature and 20 bar maximum pressure is …
Inverting the Selectivity of the Newman–Kwart Rearrangement via One Electron Oxidation at Room Temperature
SK Pedersen, A Ulfkjær, MN Newman… - The Journal of …, 2018 - ACS Publications
The discovery that the Newman–Kwart rearrangement can be performed at room
temperature by action of a simple and readily available oxidant, cerium ammonium nitrate, is …
temperature by action of a simple and readily available oxidant, cerium ammonium nitrate, is …
Development of a highly efficient single-mode microwave applicator with a resonant cavity and its application to continuous flow syntheses
S Yokozawa, N Ohneda, K Muramatsu, T Okamoto… - RSC Advances, 2015 - pubs.rsc.org
Microwave-assisted organic synthesis has many advantages and is widely applied to a
variety of reactions. We have developed a new single-mode microwave applicator, specific …
variety of reactions. We have developed a new single-mode microwave applicator, specific …