Application of microwave-assisted heterogeneous catalysis in sustainable synthesis design

A Kokel, C Schäfer, B Török - Green Chemistry, 2017 - pubs.rsc.org
An overview of recent advances, mainly focusing on the past 5–6 years, in microwave-
assisted heterogeneous catalysis is provided. The work includes three major parts;(i) a …

My twenty years in microwave chemistry: from kitchen ovens to microwaves that aren't microwaves

CO Kappe - The chemical record, 2019 - Wiley Online Library
Abstract This Personal Account describes the author's involvement in the field of microwave‐
assisted organic synthesis (MAOS) from the late 1990's starting out with kitchen microwave …

The microwave‐to‐flow paradigm: translating high‐temperature batch microwave chemistry to scalable continuous‐flow processes

TN Glasnov, CO Kappe - Chemistry–A European Journal, 2011 - Wiley Online Library
The popularity of dedicated microwave reactors in many academic and industrial
laboratories has produced a plethora of synthetic protocols that are based on this enabling …

How do the fine chemical, pharmaceutical, and related industries approach green chemistry and sustainability?

WJW Watson - Green Chemistry, 2012 - pubs.rsc.org
Developing manufacturing processes for active pharmaceutical ingredients and
intermediates often involves complex chemistry. All companies now aim to uphold the …

Microwave Flow: A Perspective on Reactor and Microwave Configurations and the Emergence of Tunable Single‐Mode Heating Toward Large‐Scale Applications

JP Barham, E Koyama, Y Norikane… - The Chemical …, 2019 - Wiley Online Library
Microwave heating in chemical reactions was first reported in 1986. There have since been
many reports employing microwave heating in organic chemistry, where microwave heating …

Continuous flow synthesis of heterocycles: A recent update on the flow synthesis of indoles

M Colella, L Degennaro, R Luisi - Molecules, 2020 - mdpi.com
Indole derivatives are among the most useful and interesting heterocycles employed in drug
discovery and medicinal chemistry. In addition, flow chemistry and flow technology are …

Single-mode microwave reactor used for continuous flow reactions under elevated pressure

M Nishioka, M Miyakawa, Y Daino… - Industrial & …, 2013 - ACS Publications
We present a flow type single-mode microwave (MW) reactor that forms a uniform
electromagnetic field along a tubular reactor (quartz glass, id 1.5 mm× 100 mm) located in …

Design and performance validation of a conductively heated sealed-vessel reactor for organic synthesis

D Obermayer, D Znidar, G Glotz, A Stadler… - The Journal of …, 2016 - ACS Publications
A newly designed robust and safe laboratory scale reactor for syntheses under sealed-
vessel conditions at 250° C maximum temperature and 20 bar maximum pressure is …

Inverting the Selectivity of the Newman–Kwart Rearrangement via One Electron Oxidation at Room Temperature

SK Pedersen, A Ulfkjær, MN Newman… - The Journal of …, 2018 - ACS Publications
The discovery that the Newman–Kwart rearrangement can be performed at room
temperature by action of a simple and readily available oxidant, cerium ammonium nitrate, is …

Development of a highly efficient single-mode microwave applicator with a resonant cavity and its application to continuous flow syntheses

S Yokozawa, N Ohneda, K Muramatsu, T Okamoto… - RSC Advances, 2015 - pubs.rsc.org
Microwave-assisted organic synthesis has many advantages and is widely applied to a
variety of reactions. We have developed a new single-mode microwave applicator, specific …