Solid-state NMR dipolar and chemical shift anisotropy recoupling techniques for structural and dynamical studies in biological systems

L Liang, Y Ji, K Chen, P Gao, Z Zhao, G Hou - Chemical Reviews, 2022 - ACS Publications
With the development of NMR methodology and technology during the past decades, solid-
state NMR (ssNMR) has become a particularly important tool for investigating structure and …

Advanced solid-state NMR methods for the elucidation of structure and dynamics of molecular, macromolecular, and supramolecular systems

SP Brown, HW Spiess - Chemical reviews, 2001 - ACS Publications
In polymer science today, much interest is focused on the controlled design of well-ordered
superstructures based on the self-assembly of carefully chosen building blocks. Of particular …

Atomic structure of the open SARS-CoV-2 E viroporin

J Medeiros-Silva, AJ Dregni, NH Somberg, P Duan… - Science …, 2023 - science.org
The envelope (E) protein of the SARS-CoV-2 virus forms cation-conducting channels in the
endoplasmic reticulum Golgi intermediate compartment (ERGIC) of infected cells. The …

Molecular structure of amyloid fibrils: insights from solid-state NMR

R Tycko - Quarterly reviews of biophysics, 2006 - cambridge.org
1. Introduction 22. Sources of structural information in solid-state NMR data 52.1 General
remarks 52.2 Chemical shifts, linewidths, and magic-angle spinning 62.3 Dipole–dipole …

High-resolution molecular structure of a peptide in an amyloid fibril determined by magic angle spinning NMR spectroscopy

CP Jaroniec, CE MacPhee, VS Bajaj… - Proceedings of the …, 2004 - National Acad Sciences
Amyloid fibrils are self-assembled filamentous structures associated with protein deposition
conditions including Alzheimer's disease and the transmissible spongiform …

Fivefold symmetric homonuclear dipolar recoupling in rotating solids: Application to double quantum spectroscopy

M Hohwy, CM Rienstra, CP Jaroniec… - The Journal of chemical …, 1999 - pubs.aip.org
We describe a new fivefold symmetric approach to homonuclear recoupling in rotating solids
that is based on rotor-synchronized, spin-lock rf irradiation of the type employed previously …

Partitioning surface ligands on nanocrystals for maximal solubility

Z Pang, J Zhang, W Cao, X Kong, X Peng - Nature communications, 2019 - nature.com
A typical colloidal nanoparticle can be viewed as a nanocrystal-ligands complex with an
inorganic single-crystalline core, the nanocrystal, bonded with a monolayer of organic …

[HTML][HTML] Dipolar recoupling in MAS spectra of biological solids

R Griffin - Nature structural biology, 1998 - nature.com
In combination with magic angle spinning, dipolar recoupling yields solid state NMR spectral
assignments and provides constraints on internuclear distances and torsion angles. The …

Membrane protein structure and dynamics from NMR spectroscopy

M Hong, Y Zhang, F Hu - Annual review of physical chemistry, 2012 - annualreviews.org
We review the current state of membrane protein structure determination using solid-state
nuclear magnetic resonance (NMR) spectroscopy. Multidimensional magic-angle-spinning …

Dynamic nuclear polarization at 9 T using a novel 250 GHz gyrotron microwave source

VS Bajaj, CT Farrar, MK Hornstein, I Mastovsky… - Journal of Magnetic …, 2011 - Elsevier
In this communication, we report enhancements of nuclear spin polarization by dynamic
nuclear polarization (DNP) in static and spinning solids at a magnetic field strength of 9T …