Progress in spray-drying of protein pharmaceuticals: Literature analysis of trends in formulation and process attributes

JT Pinto, E Faulhammer, J Dieplinger, M Dekner… - Drying …, 2021 - Taylor & Francis
Spray-drying is an inherently continuous and well-established industrial drying process. It
can accelerate manufacturing of biopharmaceuticals and vaccine products, resulting in both …

Developments in hydrogen/deuterium exchange mass spectrometry

JR Engen, T Botzanowski, D Peterle… - Analytical …, 2020 - ACS Publications
Chemistry” on HDX MS. 1 That review covered HDX MS applications from January 2012
through June 2014 and described the publications in terms of sector, geography, and topic …

Characterization of selected dietary fibers microparticles and application of the optimized formulation as a fat replacer in hazelnut spreads

RS Zamora, A Baldelli, A Pratap-Singh - Food Research International, 2023 - Elsevier
The present work demonstrates the application of the spray drying technique to produce
microparticulates of different dietary fibers with particle sizes< 10 µm. It examines their role …

Wall Materials for Encapsulating Bioactive Compounds via Spray-Drying: A Review

E Díaz-Montes - Polymers, 2023 - mdpi.com
Spray-drying is a continuous encapsulation method that effectively preserves, stabilizes, and
retards the degradation of bioactive compounds by encapsulating them within a wall …

Pharmaceutical protein solids: Drying technology, solid-state characterization and stability

Y Chen, TT Mutukuri, NE Wilson, QT Zhou - Advanced drug delivery …, 2021 - Elsevier
Despite the boom in biologics over the past decade, the intrinsic instability of these large
molecules poses significant challenges to formulation development. Almost half of all …

Understanding the impact of protein–excipient interactions on physical stability of spray-dried protein solids

Y Chen, J Ling, M Li, Y Su, KS Arte… - Molecular …, 2021 - ACS Publications
Mannitol, leucine, and trehalose have been widely used in spray-dried formulations,
especially for inhalation formulations. The individual contribution of these excipients on …

Effects of drying method and excipient on the structure and physical stability of protein solids: Freeze drying vs. spray freeze drying

TT Mutukuri, NE Wilson, LS Taylor, EM Topp… - International journal of …, 2021 - Elsevier
This study aims to determine the impacts of drying method and excipient on changes in
protein structure and physical stability of model protein solids. Protein solids containing one …

Effect of buffer salts on physical stability of lyophilized and spray-dried protein formulations containing bovine serum albumin and trehalose

TT Mutukuri, J Ling, Y Du, Y Su, QT Zhou - Pharmaceutical research, 2023 - Springer
This study examined the effect of buffer salts on the physical stability of spray-dried and
lyophilized formulations of a model protein, bovine serum albumin (BSA). BSA formulations …

Inhalable microparticle platform based on a novel shell-forming lipid excipient and its feasibility for respirable delivery of biologics

H Wang, P Connaughton, K Lachacz, N Carrigy… - European Journal of …, 2022 - Elsevier
Administration of biologics such as proteins, vaccines, and phages via the respiratory route
is becoming increasingly popular. Inhalable powder formulations for the successful delivery …

Mechanism of insoluble aggregate formation in a reconstituted solution of spray-dried protein powder

Y Tao, Y Chen, W Howard, M Ibrahim, SM Patel… - Pharmaceutical …, 2023 - Springer
Background Spray-drying is considered a promising alternative drying method to
lyophilization (freeze-drying) for therapeutic proteins. Particle counts in reconstituted …