Column characterization and selection systems in reversed-phase high-performance liquid chromatography

P Žuvela, M Skoczylas, J Jay Liu, T Ba̧czek… - Chemical …, 2019 - ACS Publications
Reversed-phase high-performance liquid chromatography (RP-HPLC) is the most popular
chromatographic mode, accounting for more than 90% of all separations. HPLC itself owes …

Development of silica-based stationary phases for high-performance liquid chromatography

H Qiu, X Liang, M Sun, S Jiang - Analytical and Bioanalytical Chemistry, 2011 - Springer
Stationary phases are the basis of the development and application of high-performance
liquid chromatography (HPLC). In this review we focused on the development of silica …

Recent advances in the direct and indirect liquid chromatographic enantioseparation of amino acids and related compounds: A review

I Ilisz, A Aranyi, Z Pataj, A Péter - Journal of pharmaceutical and biomedical …, 2012 - Elsevier
Amino acids are essential for life, and have many functions in metabolism. One particularly
important function is to serve as the building blocks of peptides and proteins, giving rise to …

Application of TLC, HPLC and GC methods to the study of amino acid and peptide enantiomers: a review

M Dołowy, A Pyka - Biomedical Chromatography, 2014 - Wiley Online Library
Amino acids are very important organic compounds in nature. The biological activity of
amino acids depends mainly on their stereoisomeric configuration (d‐or l‐). Thus, the …

Addition of lithium carbenoids to isocyanates: a direct access to synthetically useful N-substituted 2-haloacetamides

V Pace, L Castoldi, W Holzer - Chemical Communications, 2013 - pubs.rsc.org
The addition of lithium carbenoids to isocyanates provides a versatile access to N-
substituted 2-haloacetamides: the reaction tolerates the presence of variously functionalized …

Enantiomeric separation of nonproteinogenic amino acids by high-performance liquid chromatography

I Ilisz, A Aranyi, Z Pataj, A Péter - Journal of Chromatography A, 2012 - Elsevier
Amino acids are essential for life, and have many functions in metabolism. One particularly
important function is to serve as the building blocks of peptides and proteins, giving rise …

The enantiomeric differentiation ability of chiral crown ethers based on carbohydrates

P Bakó, G Keglevich, Z Rapi… - Current Organic Chemistry, 2012 - ingentaconnect.com
The enantiomeric differentiation ability of chiral sugar-based crown ethers can be utilized for
the determination of the enantiomeric composition of chiral amino compounds and for the …

Synthesis and enantiomeric recognition ability of 22-crown-6 ethers derived from rosin acid and BINOL

H Wang, X Tian, D Yang, Y Pan, Q Wu, C He - Tetrahedron: Asymmetry, 2011 - Elsevier
Four novel chiral 22-crown-6 ethers 6a–b, 7a–b bearing hydroxyl side groups derived from
rosin acid and BINOL were prepared in optically pure forms, and their enantiodiscriminating …

Synthesis and evaluation of chiral selectors with multiple hydrogen-bonding sites in the macrocyclic cavities

T Ema, K Hamada, K Sugita, Y Nagata… - The Journal of …, 2010 - ACS Publications
Chiral macrocycles with the hydrogen bond donor/acceptor sites in the cavity were
synthesized and covalently bonded to silica gel to give chiral stationary phases (CSPs) …

Preparation of a new chiral acridino-18-crown-6 ether-based stationary phase for enantioseparation of racemic protonated primary aralkyl amines

S Lakatos, J Fetter, F Bertha, P Huszthy, T Tóth… - Tetrahedron, 2008 - Elsevier
Starting from commercially available and relatively cheap chemicals first enantiopure
dimethyl-substituted monoaza-18-crown-6 ether (R, R)-21 containing a diphenylamine unit …