[HTML][HTML] Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR

ASL Thankamony, JJ Wittmann, M Kaushik… - Progress in nuclear …, 2017 - Elsevier
The field of dynamic nuclear polarization has undergone tremendous developments and
diversification since its inception more than 6 decades ago. In this review we provide an in …

Biomolecular and biological applications of solid-state NMR with dynamic nuclear polarization enhancement

WY Chow, G De Paëpe, S Hediger - Chemical Reviews, 2022 - ACS Publications
Solid-state NMR spectroscopy (ssNMR) with magic-angle spinning (MAS) enables the
investigation of biological systems within their native context, such as lipid membranes, viral …

Nuclear depolarization and absolute sensitivity in magic-angle spinning cross effect dynamic nuclear polarization

F Mentink-Vigier, S Paul, D Lee, A Feintuch… - Physical Chemistry …, 2015 - pubs.rsc.org
Over the last two decades solid state Nuclear Magnetic Resonance has witnessed a
breakthrough in increasing the nuclear polarization, and thus experimental sensitivity, with …

Theoretical aspects of magic angle spinning-dynamic nuclear polarization

F Mentink-Vigier, U Akbey, H Oschkinat, S Vega… - Journal of Magnetic …, 2015 - Elsevier
Abstract Magic Angle Spinning (MAS) combined with Dynamic Nuclear Polarization (DNP)
has been proven in recent years to be a very powerful method for increasing solid-state …

Perturbation of nuclear spin polarizations in solid state NMR of nitroxide-doped samples by magic-angle spinning without microwaves

KR Thurber, R Tycko - The Journal of chemical physics, 2014 - pubs.aip.org
We report solid state 13 C and 1 H nuclear magnetic resonance (NMR) experiments with
magic-angle spinning (MAS) on frozen solutions containing nitroxide-based paramagnetic …

Postmodification via thiol-click chemistry yields hydrophilic trityl-nitroxide biradicals for biomolecular high-field dynamic nuclear polarization

W Zhai, A Lucini Paioni, X Cai… - The Journal of …, 2020 - ACS Publications
Dynamic nuclear polarization (DNP) is a powerful method to enhance nuclear magnetic
resonance (NMR) signal intensities, enabling unprecedented applications in life and …

NMR-based structural biology enhanced by dynamic nuclear polarization at high magnetic field

EJ Koers, EAW van Der Cruijsen, M Rosay… - Journal of biomolecular …, 2014 - Springer
Dynamic nuclear polarization (DNP) has become a powerful method to enhance
spectroscopic sensitivity in the context of magnetic resonance imaging and nuclear …

19F Dynamic Nuclear Polarization at Fast Magic Angle Spinning for NMR of HIV-1 Capsid Protein Assemblies

M Lu, M Wang, IV Sergeyev, CM Quinn… - Journal of the …, 2019 - ACS Publications
We report remarkably high, up to 100-fold, signal enhancements in 19F dynamic nuclear
polarization (DNP) magic angle spinning (MAS) spectra at 14.1 T on HIV-1 capsid protein …

The magnetic field dependence of cross-effect dynamic nuclear polarization under magic angle spinning

D Mance, P Gast, M Huber, M Baldus… - The Journal of Chemical …, 2015 - pubs.aip.org
We develop a theoretical description of Dynamic Nuclear Polarization (DNP) in solids under
Magic Angle Spinning (MAS) to describe the magnetic field dependence of the DNP effect …

[HTML][HTML] Cellular solid-state NMR investigation of a membrane protein using dynamic nuclear polarization

K Yamamoto, MA Caporini, SC Im, L Waskell… - … et Biophysica Acta (BBA …, 2015 - Elsevier
While an increasing number of structural biology studies successfully demonstrate the
power of high-resolution structures and dynamics of membrane proteins in fully …