Advances and perspectives in chemical isotope labeling-based mass spectrometry methods for metabolome and exposome analysis

S Gao, X Zhou, M Yue, S Zhu, Q Liu, XE Zhao - TrAC Trends in Analytical …, 2023 - Elsevier
Metabolomics and exposomics are important in the studies of human health and diseases.
Chemical isotope labeling (CIL) combined with mass spectrometry (MS) can not only …

[HTML][HTML] Recent techniques in nutrient analysis for food composition database

MF Md Noh, RDN Gunasegavan, N Mustafa Khalid… - Molecules, 2020 - mdpi.com
Food composition database (FCD) provides the nutritional composition of foods. Reliable
and up-to date FCD is important in many aspects of nutrition, dietetics, health, food science …

[HTML][HTML] Total and free fatty acids analysis in milk and dairy fat

G Amores, M Virto - Separations, 2019 - mdpi.com
Dairy fat is one of the most complex natural fats because of its fatty acid (FA) composition.
Ruminant dairy fat contains more than 400 different FA varying in carbon chain length, and …

Magnetic ionic liquids as extraction solvents in vacuum headspace single-drop microextraction

MJ Trujillo-Rodriguez, V Pino, JL Anderson - Talanta, 2017 - Elsevier
A vacuum headspace single-drop microextraction method based on the use of magnetic
ionic liquids (vacuum MIL-HS-SDME) for the determination of short chain free fatty acids is …

Mass spectrometry-based single-cell lipidomics: Advancements, challenges, and the path forward

CE Randolph, P Manchanda, H Arora, S Iyer… - TrAC Trends in …, 2023 - Elsevier
In the past decade, lipidomics, now recognized as standalone subdiscipline of
metabolomics, has gained considerable attention. Due to its sensitivity and unparalleled …

A novel HPLC-ESI-Q-ToF approach for the determination of fatty acids and acylglycerols in food samples

J La Nasa, I Degano, L Brandolini, F Modugno… - Analytica chimica …, 2018 - Elsevier
We propose a new analytical method using reverse phase High performance liquid
chromatography (HPLC) coupled through an electrospray source with a tandem quadrupole …

Derivatization of carboxylic groups prior to their LC analysis–A review

T Jankech, I Gerhardtova, P Majerova, J Piestansky… - Analytica Chimica …, 2024 - Elsevier
Carboxylic acids (CAs) represent a large group of important molecules participating in
various biologically significant processes. Analytical study of these compounds is typically …

Current trends in isotope‐coded derivatization liquid chromatographic‐mass spectrometric analyses with special emphasis on their biomedical application

MH El‐Maghrabey, N Kishikawa… - Biomedical …, 2020 - Wiley Online Library
Currently, LC–MS has various applications in different areas such as metabolomics,
pharmacokinetics, and pathological studies. Yet, matrix effects resulting from co‐existing …

A sensitive method for the quantification of short-chain fatty acids by benzyl chloroformate derivatization combined with GC-MS

M Li, R Zhu, X Song, Z Wang, H Weng, J Liang - Analyst, 2020 - pubs.rsc.org
Short-chain fatty acids (SCFAs) were identified as critical markers in the diagnosis of chronic
and metabolic diseases, but a sensitive and stable method to determine SCFAs in feces is a …

[HTML][HTML] A rapid and sensitive profiling of free fatty acids using liquid chromatography electrospray ionization tandem mass spectrometry (LC/ESI-MS/MS) after …

HJ Mok, JW Lee, R Bandu, HS Kang, KH Kim, KP Kim - RSC advances, 2016 - pubs.rsc.org
Free fatty acids (FFAs) have diverse roles in cellular energy and signaling and they are
critical molecules in various biological states. Due to the poor ionization efficiency of FFAs …