Crystal engineering of pharmaceutical cocrystals in the discovery and development of improved drugs

G Bolla, B Sarma, AK Nangia - Chemical reviews, 2022 - ACS Publications
The subject of crystal engineering started in the 1970s with the study of topochemical
reactions in the solid state. A broad chemical definition of crystal engineering was published …

Coupling hot melt extrusion and fused deposition modeling: Critical properties for successful performance

S Bandari, D Nyavanandi, N Dumpa… - Advanced drug delivery …, 2021 - Elsevier
Interest in 3D printing for pharmaceutical applications has increased in recent years.
Compared to other 3D printing techniques, hot melt extrusion (HME)-based fused deposition …

A systematic and robust assessment of hot-melt extrusion-based amorphous solid dispersions: Theoretical prediction to practical implementation

A Alzahrani, D Nyavanandi, P Mandati… - International Journal of …, 2022 - Elsevier
Amorphous solid dispersions (ASDs) have gained attention as a formulation strategy in
recent years, with the potential to improve the apparent solubility and, hence, the oral …

Drug complexes: perspective from academic research and pharmaceutical market

SR Munnangi, AAA Youssef, N Narala… - Pharmaceutical …, 2023 - Springer
Despite numerous research efforts, drug delivery through the oral route remains a major
challenge to formulation scientists. The oral delivery of drugs poses a significant challenge …

Emerging role of nanocrystals in pharmaceutical applications: A review of regulatory aspects and drug development process

PS Chary, S Shaikh, V Bhavana, N Rajana… - Applied Materials …, 2024 - Elsevier
A significant majority of the 20 approved nanoformulations consist predominantly of
nanocrystals (NCs). NCs are nanosized drug moieties comprising 100% of the drug with …

Amorphous solid forms of ranolazine and tryptophan and their relaxation to metastable polymorphs

JFC Silva, PS Pereira Silva, M Ramos Silva… - Crystal Growth & …, 2023 - ACS Publications
Different methods were explored for the amorphization of ranolazine, a sparingly soluble
anti-anginal drug, such as mechanochemistry, quench-cooling, and solvent evaporation …

Hot-melt extrusion: from theory to application in pharmaceutical formulation—where are we now?

H Patil, SK Vemula, S Narala, P Lakkala… - AAPS …, 2024 - Springer
Hot-melt extrusion (HME) is a globally recognized, robust, effective technology that
enhances the bioavailability of poorly soluble active pharmaceutical ingredients and offers …

[HTML][HTML] Solid-state and particle size control of pharmaceutical cocrystals using atomization-based techniques

A O'Sullivan, B Long, V Verma, KM Ryan… - International Journal of …, 2022 - Elsevier
Poor bioavailability and aqueous solubility represent a major constraint during the
development of new API molecules and can influence the impact of new medicines or halt …

Creation of hydrochlorothiazide pharmaceutical cocrystals via hot-melt extrusion for enhanced solubility and permeability

S Narala, D Nyavanandi, A Alzahrani, S Bandari… - AAPS …, 2022 - Springer
Crystal engineering is an emerging tool for altering the physicochemical properties of drug
candidates. The objective of the current investigation was to develop cocrystals of …

Feasibility of high melting point hydrochlorothiazide processing via cocrystal formation by hot melt extrusion paired fused filament fabrication as a 3D-printed cocrystal …

D Nyavanandi, P Mandati, S Narala, A Alzahrani… - International Journal of …, 2022 - Elsevier
The development of amorphous solid dispersions (ASDs) of high-melting-point drug
substances using hot-melt extrusion (HME) continues to be challenging because of the …