Ultrafast magic angle spinning solid-state NMR spectroscopy: Advances in methodology and applications

Y Nishiyama, G Hou, V Agarwal, Y Su… - Chemical …, 2022 - ACS Publications
Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …

1H-Detected Biomolecular NMR under Fast Magic-Angle Spinning

T Le Marchand, T Schubeis, M Bonaccorsi… - Chemical …, 2022 - ACS Publications
Since the first pioneering studies on small deuterated peptides dating more than 20 years
ago, 1H detection has evolved into the most efficient approach for investigation of …

Solid-state NMR: Methods for biological solids

S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …

From angstroms to nanometers: measuring interatomic distances by solid-state NMR

AA Shcherbakov, J Medeiros-Silva, N Tran… - Chemical …, 2021 - ACS Publications
Internuclear distances represent one of the main structural constraints in molecular structure
determination using solid-state NMR spectroscopy, complementing chemical shifts and …

Broadband homonuclear correlation spectroscopy driven by combined R2nv sequences under fast magic angle spinning for NMR structural analysis of organic and …

G Hou, S Yan, J Trebosc, JP Amoureux… - Journal of Magnetic …, 2013 - Elsevier
We recently described a family of experiments for R2nv Driven Spin Diffusion (RDSD)
spectroscopy suitable for homonuclear correlation experiments under fast MAS conditions …

[PDF][PDF] Solid-state NMR and EPR methods for metal ion battery research

C Li, M Shen, B Hu - Acta Phys. Chim. Sin, 2020 - whxb.pku.edu.cn
The rapid development of batteries, especially lithium-ion batteries, has dramatically
changed our daily lives. From portable electronics to electric vehicles and smart grids …

Mixing Aβ (1–40) and Aβ (1–42) peptides generates unique amyloid fibrils

L Cerofolini, E Ravera, S Bologna… - Chemical …, 2020 - pubs.rsc.org
Recent structural studies show distinct morphologies for the fibrils of Aβ (1–42) and Aβ (1–
40), which are believed not to co-fibrillize. We describe here a novel, structurally-uniform 1: 1 …

Protein structure determination by magic-angle spinning solid-state NMR, and insights into the formation, structure, and stability of amyloid fibrils

G Comellas, CM Rienstra - Annual review of biophysics, 2013 - annualreviews.org
Protein structure determination methods using magic-angle spinning solid-state nuclear
magnetic resonance (MAS SSNMR) have experienced a remarkable development in the …

Application of solid-state NMR techniques for structural characterization of metal-organic frameworks

C He, S Li, Y Xiao, J Xu, F Deng - Solid State Nuclear Magnetic Resonance, 2022 - Elsevier
Solid-state NMR can afford the structural information about the chemical composition, local
environment, and spatial coordination at the atomic level, which has been extensively …

[HTML][HTML] Advanced solid-state NMR spectroscopy and its applications in zeolite chemistry

M Zheng, Y Chu, Q Wang, Y Wang, J Xu… - Progress in Nuclear …, 2023 - Elsevier
Solid-state NMR spectroscopy (ssNMR) can provide details about the structure, host-
guest/guest-guest interactions and dynamic behavior of materials at atomic length scales. A …