1H-Detected Biomolecular NMR under Fast Magic-Angle Spinning

T Le Marchand, T Schubeis, M Bonaccorsi… - Chemical …, 2022 - ACS Publications
Since the first pioneering studies on small deuterated peptides dating more than 20 years
ago, 1H detection has evolved into the most efficient approach for investigation of …

Solid-state NMR: Methods for biological solids

S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …

Understanding fluoroethylene carbonate and vinylene carbonate based electrolytes for Si anodes in lithium ion batteries with NMR spectroscopy

Y Jin, NJH Kneusels, LE Marbella… - Journal of the …, 2018 - ACS Publications
Fluoroethylene carbonate (FEC) and vinylene carbonate (VC) are widely used as electrolyte
additives in lithium ion batteries. Here we analyze the solid electrolyte interphase (SEI) …

Fluoroethylene carbonate and vinylene carbonate reduction: understanding lithium-ion battery electrolyte additives and solid electrolyte interphase formation

AL Michan, BS Parimalam, M Leskes… - Chemistry of …, 2016 - ACS Publications
We have synthesized the products of fluoroethylene carbonate (FEC) and vinylene
carbonate (VC) via lithium naphthalenide reduction. By analyzing the resulting solid …

Identifying the structural basis for the increased stability of the solid electrolyte interphase formed on silicon with the additive fluoroethylene carbonate

Y Jin, NJH Kneusels, PCMM Magusin… - Journal of the …, 2017 - ACS Publications
To elucidate the role of fluoroethylene carbonate (FEC) as an additive in the standard
carbonate-based electrolyte for Li-ion batteries, the solid electrolyte interphase (SEI) formed …

Solid electrolyte interphase growth and capacity loss in silicon electrodes

AL Michan, G Divitini, AJ Pell, M Leskes… - Journal of the …, 2016 - ACS Publications
The solid electrolyte interphase (SEI) of the high capacity anode material Si is monitored
over multiple electrochemical cycles by 7Li, 19F, and 13C solid-state nuclear magnetic …

Conformational fitting of a flexible oligomeric substrate does not explain the enzymatic PET degradation

R Wei, C Song, D Gräsing, T Schneider… - Nature …, 2019 - nature.com
Methods Solid-state NMR analysis of amorphous PET powder. Amorphous PET films
(product no. ES301445) were purchased from Goodfellow Cambridge Ltd.(Huntingdon, UK) …

Voltage dependent solid electrolyte interphase formation in silicon electrodes: monitoring the formation of organic decomposition products

AL Michan, M Leskes, CP Grey - Chemistry of Materials, 2016 - ACS Publications
The solid electrolyte interphase (SEI) passivating layer that grows on all battery electrodes
during cycling is critical to the long-term capacity retention of lithium-ion batteries. Yet, it is …

Spinning faster: protein NMR at MAS frequencies up to 126 kHz

S Penzel, A Oss, ML Org, A Samoson… - Journal of biomolecular …, 2019 - Springer
We report linewidth and proton T 1, T 1 ρ and T 2′ relaxation data of the model protein
ubiquitin acquired at MAS frequencies up to 126 kHz. We find a predominantly linear …

On the binding mode and molecular mechanism of enzymatic polyethylene terephthalate degradation

P Falkenstein, Z Zhao, A Di Pede-Mattatelli… - ACS …, 2023 - ACS Publications
Enzymatic degradation of polyethylene terephthlate (PET) by polyester hydrolases is
currently subject to intensive research, as it is considered as a potential eco-friendly …