Heteronuclear multidimensional NMR experiments for the structure determination of proteins in solution employing pulsed field gradients

M Sattler, J Schleucher, C Griesinger - Progress in nuclear magnetic …, 1999 - Elsevier
6. 3D and 4D NOESY/ROESY experiments............................................ 146 6.1. 13C-and 15N-
edited NOESY/ROESY experiments.................................. 146 6.2. Filtered experiments for …

Determination of relative configuration in organic compounds by NMR spectroscopy and computational methods

G Bifulco, P Dambruoso, L Gomez-Paloma… - Chemical …, 2007 - ACS Publications
Stereochemical features have a profound impact on a variety of molecular properties, such
as chemical reactivity and catalytic, biological, and pharmacological activities. In light of the …

[图书][B] High-resolution NMR techniques in organic chemistry

TDW Claridge - 2016 - books.google.com
High-Resolution NMR Techniques in Organic Chemistry, Third Edition describes the most
important NMR spectroscopy techniques for the structure elucidation of organic molecules …

Gradient-tailored excitation for single-quantum NMR spectroscopy of aqueous solutions

M Piotto, V Saudek, V Sklenář - Journal of biomolecular NMR, 1992 - Springer
A novel approach to tailored selective excitation for the measurement of NMR spectra in non-
deuterated aqueous solutions (WATERGATE, WATER suppression by GraAdient-Tailored …

Pure absorption gradient enhanced heteronuclear single quantum correlation spectroscopy with improved sensitivity

L Kay, P Keifer, T Saarinen - Journal of the American Chemical …, 1992 - ACS Publications
Figure 1. Pulse sequence of the sensitivity enhanced gradient'H-15N HSQC experiment.
Narrow pulses represent a flip angle of 90 with wider pulses representing a flip angle of 180 …

[图书][B] Lignin and lignans: advances in chemistry

C Heitner, D Dimmel, J Schmidt - 2016 - books.google.com
Over the past four decades, there has been immense progress in every area of lignin
science, ranging from the enzymology of lignin biodegradation, to the delignification of wood …

A general enhancement scheme in heteronuclear multidimensional NMR employing pulsed field gradients

J Schleucher, M Schwendinger, M Sattler… - Journal of biomolecular …, 1994 - Springer
General pulse sequence elements that achieve sensitivity-enhanced coherence transfer
from a heteronucleus to protons of arbitrary multiplicity are introduced. The building blocks …

Gradient selection in inverse heteronuclear correlation spectroscopy

W Willker, D Leibfritz, R Kerssebaum… - Magnetic Resonance …, 1993 - Wiley Online Library
After a brief theoretical description, new gradient‐selected, proton‐detected heteronuclear
correlation sequences are introduced. The gs‐HMBC and gs‐Relayed‐HMQC are closely …

THE USE OF 2H, 13C, 15N MULTIDIMENSIONAL NMR GTO STUDY THE STRUCTURE AND DYNAMICS OF PROTEINS

KH Gardner, LE Kay - Annual review of biophysics and …, 1998 - annualreviews.org
▪ Abstract During the past thirty years, deuterium labeling has been used to improve the
resolution and sensitivity of protein NMR spectra used in a wide variety of applications. Most …

Location and properties of metal-binding sites on the human prion protein

GS Jackson, I Murray, LLP Hosszu… - Proceedings of the …, 2001 - National Acad Sciences
Although a functional role in copper binding has been suggested for the prion protein,
evidence for binding at affinities characteristic of authentic metal-binding proteins has been …