Single-crystal structure determination of nanosized metal–organic frameworks by three-dimensional electron diffraction

T Yang, T Willhammar, H Xu, X Zou, Z Huang - Nature Protocols, 2022 - nature.com
Metal–organic frameworks (MOFs) have attracted considerable interest due to their well-
defined pore architecture and structural tunability on molecular dimensions. While single …

3D electron diffraction for chemical analysis: Instrumentation developments and innovative applications

T Gruene, E Mugnaioli - Chemical Reviews, 2021 - ACS Publications
In the past few years, many exciting papers reported results based on crystal structure
determination by electron diffraction. The aim of this review is to provide general and …

Accurate structure models and absolute configuration determination using dynamical effects in continuous-rotation 3D electron diffraction data

PB Klar, Y Krysiak, H Xu, G Steciuk, J Cho, X Zou… - Nature Chemistry, 2023 - nature.com
Continuous-rotation 3D electron diffraction methods are increasingly popular for the
structure analysis of very small organic molecular crystals and crystalline inorganic …

Revolutionizing the structural design and determination of covalent–organic frameworks: principles, methods, and techniques

Y Liu, X Liu, A Su, C Gong, S Chen, L Xia… - Chemical Society …, 2024 - pubs.rsc.org
Covalent organic frameworks (COFs) represent an important class of crystalline porous
materials with designable structures and functions. The interconnected organic monomers …

Structure and function tailored metal-organic frameworks for heterogeneous catalysis

G Zhou, Y Wang, Z Huang - Chem Catalysis, 2022 - cell.com
The unlimited combination of building units, tunable structures, and facilitation of tailoring
active sites endows metal-organic frameworks (MOFs) with high activity as heterogeneous …

Catching a new zeolite as a transition material during deconstruction

Q Yue, G Steciuk, M Mazur, J Zhang… - Journal of the …, 2023 - ACS Publications
Zeolites are key materials in both basic research and industrial applications. However, their
synthesis is neither diverse nor applicable to labile frameworks because classical …

Direct location of organic molecules in framework materials by three-dimensional electron diffraction

M Ge, T Yang, H Xu, X Zou… - Journal of the American …, 2022 - ACS Publications
In the study of framework materials, probing interactions between frameworks and organic
molecules is one of the most important tasks, which offers us a fundamental understanding …

[PDF][PDF] Accurate lattice parameters from 3D electron diffraction data. I. Optical distortions

P Brázda, M Klementová, Y Krysiak, L Palatinus - IUCrJ, 2022 - journals.iucr.org
Determination of lattice parameters from 3D electron diffraction (3D ED) data measured in a
transmission electron microscope is hampered by a number of effects that seriously limit the …

[PDF][PDF] STEM SerialED: achieving high-resolution data for ab initio structure determination of beam-sensitive nanocrystalline materials

P Hogan-Lamarre, Y Luo, R Bücker, RJD Miller, X Zou - IUCrJ, 2024 - journals.iucr.org
Serial electron diffraction (SerialED), which applies a snapshot data acquisition strategy for
each crystal, was introduced to tackle the problem of radiation damage in the structure …

The elusive structure of magadiite, solved by 3D electron diffraction and model building

Y Krysiak, M Maslyk, BN Silva, S Plana-Ruiz… - Chemistry of …, 2021 - ACS Publications
In addition to a great swelling ability, layered silicates also allow the functionalization of their
interlayer region to form various robust green materials that are used as CO2 adsorbents …