A review of infrared spectroscopy in microarchaeology: Methods, applications, and recent trends

GF Monnier - Journal of Archaeological Science: Reports, 2018 - Elsevier
Infrared (IR) spectroscopy has emerged as one of the most powerful analytical tools
available to archaeologists. It has been used to document site formation processes and …

Heat treatment in the South African Middle Stone Age: temperature induced transformations of silcrete and their technological implications

P Schmidt, G Porraz, A Slodczyk, L Bellot-Gurlet… - Journal of …, 2013 - Elsevier
It was recently found that silcrete raw material was heat-treated during the South African
Middle Stone Age (MSA) for altering its flaking properties. This finding led to hypotheses …

Crystallographic and structural transformations of sedimentary chalcedony in flint upon heat treatment

P Schmidt, S Masse, G Laurent, A Slodczyk… - Journal of …, 2012 - Elsevier
The early occurrence of intentional heat treatment of silica rocks has recently become a key
element in the discussion about the cultural modernity of prehistoric populations. Lithic …

Investigation of silica polymorphs stratified in siliceous geode using FTIR and XRD methods

SM Awadh, ZM Yaseen - Materials Chemistry and Physics, 2019 - Elsevier
The study aims to differentiate the silica forms stratified in the siliceous geodes using
infrared spectroscopy (FTIR) and X-ray diffraction (XRD). The water content (total water, H 2 …

In situ analysis of opal in Gale Crater, Mars

W Rapin, B Chauviré, TSJ Gabriel… - Journal of …, 2018 - Wiley Online Library
Silica enrichments resulting in up to~ 90 wt% SiO2 have been observed by the Curiosity
rover's instruments in Gale crater, Mars, within the Murray and Stimson formations. Samples …

Detailed FT near-infrared study of the behaviour of water and hydroxyl in sedimentary length-fast chalcedony, SiO2, upon heat treatment

P Schmidt, A Badou, F Fröhlich - … Acta Part A: Molecular and Biomolecular …, 2011 - Elsevier
Chalcedony is a porous spatial arrangement of hydroxylated nanometre sized α-quartz
(SiO2) crystallites. Due to micro-structural transformations upon heat treatment, the optical …

Thermal analysis by variable temperature infrared spectroscopy with a button sample holder and peltier heating/cooling

RL White - Talanta, 2023 - Elsevier
An apparatus and methodology for variable temperature infrared spectroscopy
measurements of neat samples contained in a button sample holder are described. Sample …

The mineralogy and structure of use-wear polish on chert

P Schmidt, A Rodriguez, K Yanamandra, RK Behera… - Scientific reports, 2020 - nature.com
Polished edges of archaeological stone tools are commonly investigated to obtain
information on the tools' uses in prehistory. Yet to this day, it remains unclear what exactly …

Moganite detection in silica rocks using Raman and infrared spectroscopy

P Schmidt, L Bellot-Gurlet, V Léa… - European Journal of …, 2013 - pubs.geoscienceworld.org
The quantitative determination of moganite in flint and chert plays an important role in the
characterisation of these silica rocks and in the study of their genesis and evolution. Both …

Study of the thermal treatment of SiO2 aggregate

N Tahiri, L Khouchaf, M Elaatmani… - IOP Conference …, 2014 - iopscience.iop.org
Crystalline quality and the silanoles defects (Si-OH) present within the structure of natural
SiO 2 play an important role in its reactivity. In this work, the relationship between the loss of …