XRD and FTIR crystallinity indices in sound human tooth enamel and synthetic hydroxyapatite

J Reyes-Gasga, EL Martínez-Piñeiro… - Materials Science and …, 2013 - Elsevier
The crystallinity index (CI) is a measure of the percentage of crystalline material in a given
sample and it is also correlated to the degree of order within the crystals. In the literature two …

Sintering behaviour of natural porous hydroxyapatite derived from bovine bone

A Niakan, S Ramesh, P Ganesan, CY Tan… - Ceramics …, 2015 - Elsevier
The aim of this research is to study the properties of natural porous hydroxyapatite
developed from bovine bone through a sintering process. Bovine bone samples were …

Role of ion substitution and lattice water in the densification of cold-sintered hydroxyapatite

HZ Shen, N Guo, L Zhao, P Shen - Scripta Materialia, 2020 - Elsevier
High-density hydroxyapatite (HA) compacts were achieved by cold sintering of co-
precipitated powders at temperatures lower than 200° C without addition of any solvent …

In situ mineralized hydroxyapatite on amino acid modified nanoclays as novel bone biomaterials

A Ambre, KS Katti, DR Katti - Materials Science and Engineering: C, 2011 - Elsevier
A novel biomineralization route to synthesis of hydroxyapatite (HAP) in montmorillonite
(MMT) clay galleries modified with 5-aminovaleric acid is presented. The oraganomodified …

Structural Water in Carbonated Hydroxylapatite and Fluorapatite: Confirmation by Solid State 2H NMR

CH Yoder, JD Pasteris, KN Worcester… - Calcified Tissue …, 2012 - Springer
Water is well recognized as an important component in bone, typically regarded as a
constituent of collagen, a pore-filling fluid in bone, and an adsorbed species on the surface …

The investigation of some physical properties and microstructure of Zn-doped hydroxyapatite bioceramics prepared by sol–gel method

O Kaygili, C Tatar - Journal of sol-gel science and technology, 2012 - Springer
In this study, the effect of Zn-dopant on the physical properties and microstructure of
hydroxyapatite (HAP) bioceramics was investigated. The average crystallite size, phase …

Temperature-related changes of Ca and P release in synthesized hydroxylapatite, geological fluorapatite, and bone bioapatite

W Chen, Q Wang, S Meng, P Yang, L Jiang, X Zou… - Chemical …, 2017 - Elsevier
Solubility of apatite is highly addressed in mineralogical and material studies. Heating is one
of the major processes in apatite industry. In this study, synthesized hydroxylapatite (HAp) …

X-ray diffraction and in situ pressurization of dentine apatite reveals nanocrystal modulus stiffening upon carbonate removal

JB Forien, J Uzuhashi, T Ohkubo, K Hono, L Luo… - Acta Biomaterialia, 2021 - Elsevier
Bone-like materials comprise carbonated-hydroxyapatite nanocrystals (c-Ap) embedding a
fibrillar collagen matrix. The mineral particles stiffen the nanocomposite by tight attachment …

Structural and dielectrical properties of Mg3–Ca3 (PO4) 2 bioceramics obtained from hydroxyapatite by sol–gel method

O Kaygili, C Tatar, F Yakuphanoglu - Ceramics International, 2012 - Elsevier
Mg3–Ca3 (PO4) 2 bioceramics were prepared from hydroxyapatite (HAp) with high Mg
contents using sol–gel method. The influence of magnesium on the phase composition …

Photoacoustic FTIR spectroscopic study of undisturbed human cortical bone

C Gu, DR Katti, KS Katti - Spectrochimica Acta Part A: Molecular and …, 2013 - Elsevier
Chemical pretreatment has been the prevailing sample preparation procedure for infrared
(IR) spectroscopic studies on bone. However, experiments have indicated that chemical …