Solid-state NMR: Methods for biological solids
S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …
transformed from a spectroscopic technique investigating small molecules and industrial …
Hybridizing cross-polarization with NOE or refocused-INEPT enhances the sensitivity of MAS NMR spectroscopy
Heteronuclear cross polarization (CP) has been commonly used to enhance the sensitivity
of dilute low-γ nuclei in almost all solid-state NMR experiments. However, CP relies on …
of dilute low-γ nuclei in almost all solid-state NMR experiments. However, CP relies on …
Utilizing afterglow magnetization from cross-polarization magic-angle-spinning solid-state NMR spectroscopy to obtain simultaneous heteronuclear multidimensional …
JR Banigan, NJ Traaseth - The journal of physical chemistry B, 2012 - ACS Publications
The time required for data acquisition and subsequent spectral assignment are limiting
factors for determining biomolecular structure and dynamics using solid-state NMR …
factors for determining biomolecular structure and dynamics using solid-state NMR …
Rapid convergence of optimal control in NMR using numerically-constructed toggling frames
We present a numerical method for rapidly solving the Bloch equation for an arbitrary time-
varying spin-1/2 Hamiltonian. The method relies on fast, vectorized computations such as …
varying spin-1/2 Hamiltonian. The method relies on fast, vectorized computations such as …
Pulse design for broadband correlation NMR spectroscopy by multi-rotating frames
We present a method for designing radio-frequency (RF) pulses for broadband or multi-band
isotropic mixing at low power, suitable for protein NMR spectroscopy. These mixing pulses …
isotropic mixing at low power, suitable for protein NMR spectroscopy. These mixing pulses …
Asymmetric simultaneous phase-inversion cross-polarization in solid-state MAS NMR: Relaxing selective polarization transfer condition between two dilute spins
Double cross polarization (DCP) has been widely used for heteronuclear polarization
transfer between 13 C and 15 N in solid-state magic-angle spinning (MAS) NMR. However …
transfer between 13 C and 15 N in solid-state magic-angle spinning (MAS) NMR. However …
Band-selective heteronuclear dipolar recoupling with dual back-to-back pulses in rotating solids
Z Zhang, Y Chen, J Yang - Journal of Magnetic Resonance, 2016 - Elsevier
We propose a robust band-selective heteronuclear 15 N-13 C recoupling method using dual
back-to-back (BABA) pulses (DBP). It contains four 90° pulses in each rotor period and …
back-to-back (BABA) pulses (DBP). It contains four 90° pulses in each rotor period and …
A robust heteronuclear dipolar recoupling method comparable to TEDOR for proteins in magic-angle spinning solid-state NMR
In this letter, we propose a robust heteronuclear dipolar recoupling method for proteins in
magic-angle spinning (MAS) solid-state NMR. This method is as simple, robust and efficient …
magic-angle spinning (MAS) solid-state NMR. This method is as simple, robust and efficient …
MAS solid state NMR of proteins: simultaneous 15N–13CA and 15N–13CO dipolar recoupling via low-power symmetry-based RF pulse schemes
C Herbst, P Bellstedt, M Görlach… - Journal of Biomolecular …, 2015 - Springer
The generation of efficient RN n ν s, ν k symmetry-based low-power RF pulse schemes for
simultaneous 15 N–13 CA and 15 N–13 CO dipolar recoupling is demonstrated. The …
simultaneous 15 N–13 CA and 15 N–13 CO dipolar recoupling is demonstrated. The …
Nuclear spin relaxation in liquids and gases
J Kowalewski - 2013 - books.rsc.org
This report reviews the progress in the field of NMR relaxation in fluids. The emphasis is on
comparatively simple liquids and solutions of physico-chemical and chemical interest, in …
comparatively simple liquids and solutions of physico-chemical and chemical interest, in …