Carbohydrate structural determination by NMR spectroscopy: modern methods and limitations
JØ Duus, CH Gotfredsen, K Bock - Chemical reviews, 2000 - ACS Publications
Carbohydrates play key roles in biological recognition processes, 1, 2 in development of
diseases, 3 and in many important areas of food and technical industry. The function of …
diseases, 3 and in many important areas of food and technical industry. The function of …
Determination of relative configuration in organic compounds by NMR spectroscopy and computational methods
G Bifulco, P Dambruoso, L Gomez-Paloma… - Chemical …, 2007 - ACS Publications
Stereochemical features have a profound impact on a variety of molecular properties, such
as chemical reactivity and catalytic, biological, and pharmacological activities. In light of the …
as chemical reactivity and catalytic, biological, and pharmacological activities. In light of the …
Total Structure Determination of Apratoxin A, a Potent Novel Cytotoxin from the Marine Cyanobacterium Lyngbya majuscula
H Luesch, WY Yoshida, RE Moore… - Journal of the …, 2001 - ACS Publications
Apratoxin A (1), a potent cytotoxin with a novel skeleton, has been isolated from the marine
cyanobacterium Lyngbya majuscula Harvey ex Gomont. This cyclodepsipeptide of mixed …
cyanobacterium Lyngbya majuscula Harvey ex Gomont. This cyclodepsipeptide of mixed …
Sesquiterpene coumarins from Ferula szowitsiana and in vitro antileishmanial activity of 7-prenyloxycoumarins against promastigotes
Two new sesquiterpene coumarins, named szowitsiacoumarin A (1) and szowitsiacoumarin
B (2), and a phenylpropanoid derivative, 2-epihelmanticine (3), together with nine known …
B (2), and a phenylpropanoid derivative, 2-epihelmanticine (3), together with nine known …
Residual dipolar couplings (RDCs) in organic structure determination
CM Thiele - European Journal of Organic Chemistry, 2008 - Wiley Online Library
After the huge impact that residual dipolar couplings (RDCs) have had on the structure
determination of biological macromolecules by NMR spectroscopy, their utility in the …
determination of biological macromolecules by NMR spectroscopy, their utility in the …
Survey of NMR experiments for the determination of nJ(C,H) heteronuclear coupling constants in small molecules
BL Marquez, WH Gerwick… - Magnetic Resonance …, 2001 - Wiley Online Library
A survey of heteronuclear correlation experiments for the measurement of heteronuclear
coupling constants is presented. The purpose of this survey is to evaluate several recent …
coupling constants is presented. The purpose of this survey is to evaluate several recent …
Use of RDCs in rigid organic compounds and some practical considerations concerning alignment media
CM Thiele - Concepts in Magnetic Resonance Part A: An …, 2007 - Wiley Online Library
A molecule that is introduced into a liquid crystal or alignment medium forfeits its isotropic
tumbling motion. The resulting partial alignment leads to observable anisotropic interactions …
tumbling motion. The resulting partial alignment leads to observable anisotropic interactions …
Celebesides A− C and theopapuamides B− D, depsipeptides from an Indonesian sponge that inhibit HIV-1 entry
A Plaza, G Bifulco, JL Keffer, JR Lloyd… - The Journal of …, 2009 - ACS Publications
Six new depsipeptides belonging to two different structural classes, termed celebesides A−
C and theopapuamides B− D, have been isolated from the marine sponge Siliquariaspongia …
C and theopapuamides B− D, have been isolated from the marine sponge Siliquariaspongia …
Sensitivity enhancement of a two-dimensional experiment for the measurement of heteronuclear long range coupling constants, by a new scheme of coherence …
DO Cicero, G Barbato, R Bazzo - Journal of Magnetic Resonance, 2001 - art.torvergata.it
In this work we present a new pulse sequence for the measurement of long-range
heteronuclear coupling constants in which the optimization of coherence selection by pulsed …
heteronuclear coupling constants in which the optimization of coherence selection by pulsed …
Halipeptins A and B: Two Novel Potent Anti-inflammatory Cyclic Depsipeptides from the Vanuatu Marine Sponge Haliclona species
A Randazzo, G Bifulco, C Giannini… - Journal of the …, 2001 - ACS Publications
Two new metabolites, named halipeptins A and B, have been isolated from the marine
sponge Haliclona sp. Their structures were determined by extensive use of one-and two …
sponge Haliclona sp. Their structures were determined by extensive use of one-and two …