Advances and new directions in crystallization control

ZK Nagy, RD Braatz - Annual review of chemical and …, 2012 - annualreviews.org
The academic literature on and industrial practice of control of solution crystallization
processes have seen major advances in the past 15 years that have been enabled by …

Polymorphism and solvatomorphism 2010

HG Brittain - Journal of pharmaceutical sciences, 2012 - Elsevier
Papers and patents that deal with polymorphism (crystal systems for which a substance can
exist in structures defined by different unit cells and where each of the forms has the same …

[图书][B] Handbook of green analytical chemistry

M de la Guardia, S Garrigues - 2012 - Wiley Online Library
Now it is time to move from the general principles to the practice. The efforts made by the
analytical chemistry and chemistry community opinion during the 2011 International Year of …

Application of PAT-based feedback control approaches in pharmaceutical crystallization

Y Gao, T Zhang, Y Ma, F Xue, Z Gao, B Hou, J Gong - Crystals, 2021 - mdpi.com
Crystallization is one of the important unit operations for the separation and purification of
solid products in the chemical, pharmaceutical, and pesticide industries, especially for …

Process systems engineering tools in the pharmaceutical industry

GM Troup, C Georgakis - Computers & Chemical Engineering, 2013 - Elsevier
The purpose of this paper is to provide a summary of the current state of the application of
process systems engineering tools in the pharmaceutical industry. In this paper, we present …

The preparation of higher performance solid form of DATNBI based on rapid in-situ solvate-mediated phase transition mechanism

Y Wang, D Han, X Zhou, Z Zhang, J Gong, H Li… - Chemical Engineering …, 2023 - Elsevier
Using energetic materials (EMs) products with impure solid forms in practical application
scenarios will lead to a series of serious consequences in terms of safety, mechanics …

In situ monitoring of polymorphic transformations using a composite sensor array of Raman, NIR, and ATR-UV/vis spectroscopy, FBRM, and PVM for an intelligent …

E Simone, AN Saleemi, ZK Nagy - Organic Process Research & …, 2015 - ACS Publications
Raman spectroscopy, particle vision and measurement (PVM), and infrared spectroscopy
have already been used singularly to detect nucleation and polymorphic transformations …

Supersaturation tracking for the development, optimization and control of crystallization processes

M Barrett, M McNamara, HX Hao, P Barrett… - … Research and Design, 2010 - Elsevier
Supersaturation is the key driving force in crystallization operations, determining nucleation
and growth kinetics, and heavily influencing physical mechanisms such as agglomeration …

Enhancing crystalline properties of a cardiovascular active pharmaceutical ingredient using a process analytical technology based crystallization feedback control …

AN Saleemi, G Steele, NI Pedge, A Freeman… - International journal of …, 2012 - Elsevier
Pharmaceutical regulatory bodies require minimal presence of solvent in an active
pharmaceutical ingredient (API) after crystallization. From a processing point of view bigger …

Monitoring of the combined cooling and antisolvent crystallisation of mixtures of aminobenzoic acid isomers using ATR-UV/vis spectroscopy and FBRM

AN Saleemi, CD Rielly, ZK Nagy - Chemical engineering science, 2012 - Elsevier
During the manufacturing of active pharmaceutical ingredients crystalline products in the
purest forms are required. Quite often multiple components are present during …
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