Solid-state NMR: Methods for biological solids
S Ahlawat, KR Mote, NA Lakomek… - Chemical Reviews, 2022 - ACS Publications
In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …
transformed from a spectroscopic technique investigating small molecules and industrial …
Probing quadrupolar nuclei by solid-state NMR spectroscopy: recent advances
C Fernandez, M Pruski - Solid State NMR, 2012 - Springer
Solid-state nuclear magnetic resonance (NMR) of quadrupolar nuclei has recently
undergone remarkable development of capabilities for obtaining structural and dynamic …
undergone remarkable development of capabilities for obtaining structural and dynamic …
Ultra-high resolution in MAS solid-state NMR of perdeuterated proteins: implications for structure and dynamics
B Reif - Journal of magnetic resonance, 2012 - Elsevier
High resolution proton spectra are obtained in MAS solid-state NMR in case samples are
prepared using perdeuterated protein and D2O in the recrystallization buffer. Deuteration …
prepared using perdeuterated protein and D2O in the recrystallization buffer. Deuteration …
Ultrafast magic angle spinning nuclear magnetic resonance
M Deschamps - Annual reports on NMR spectroscopy, 2014 - Elsevier
Recent advances in magic angle spinning (MAS) now allow spinning frequencies of 40 to
110 kHz to be reached. Ultrafast MAS is achieved in rotors with diameters smaller than …
110 kHz to be reached. Ultrafast MAS is achieved in rotors with diameters smaller than …
2 H-DNP-enhanced 2 H–13C solid-state NMR correlation spectroscopy
Perdeuteration of biological macromolecules for magic angle spinning solid-state NMR
spectroscopy can yield high-resolution 2H–13C correlation spectra and the method is …
spectroscopy can yield high-resolution 2H–13C correlation spectra and the method is …
Implementation of High Resolution 43Ca Solid State NMR Spectroscopy: Toward the Elucidation of Calcium Sites in Biological Materials
D Laurencin, C Gervais, A Wong… - Journal of the …, 2009 - ACS Publications
Calcium is one of the most abundant cations in living organisms. It is found in the mineral
phase of bone and in proteins like calmodulin. However, its exact environment beyond the …
phase of bone and in proteins like calmodulin. However, its exact environment beyond the …
Advances in instrumentation and methodology for solid-state NMR of biological assemblies
Many advances in instrumentation and methodology have furthered the use of solid-state
NMR as a technique for determining the structures and studying the dynamics of molecules …
NMR as a technique for determining the structures and studying the dynamics of molecules …
Fluid flow dynamics in MAS systems
D Wilhelm, A Purea, F Engelke - Journal of Magnetic Resonance, 2015 - Elsevier
The turbine system and the radial bearing of a high performance magic angle spinning
(MAS) probe with 1.3 mm-rotor diameter has been analyzed for spinning rates up to 67 kHz …
(MAS) probe with 1.3 mm-rotor diameter has been analyzed for spinning rates up to 67 kHz …
Indirect high-resolution detection for quadrupolar spin-3/2 nuclei in dipolar HMQC solid-state NMR experiments
J Trébosc, O Lafon, B Hu, JP Amoureux - Chemical Physics Letters, 2010 - Elsevier
We present a new kind of NMR pulse sequences to observe heteronuclear correlation
(HETCOR) specifically between spin-1/2 and spin-3/2 nuclei with isotropic resolution on the …
(HETCOR) specifically between spin-1/2 and spin-3/2 nuclei with isotropic resolution on the …
Accurate Determination of 1H‐15N Dipolar Couplings Using Inaccurate Settings of the Magic Angle in Solid‐State NMR Spectroscopy
Magic‐angle spinning (MAS) is an essential ingredient in a wide variety of solid‐state NMR
experiments. The standard procedures to adjust the rotor angle are not highly accurate …
experiments. The standard procedures to adjust the rotor angle are not highly accurate …