Recent developments in deuterium solid-state NMR for the detection of slow motions in proteins

L Vugmeyster - Solid state nuclear magnetic resonance, 2021 - Elsevier
Slow timescale dynamics in proteins are essential for a variety of biological functions
spanning ligand binding, enzymatic catalysis, protein folding and misfolding regulations, as …

Probing quadrupolar nuclei by solid-state NMR spectroscopy: recent advances

C Fernandez, M Pruski - Solid State NMR, 2012 - Springer
Solid-state nuclear magnetic resonance (NMR) of quadrupolar nuclei has recently
undergone remarkable development of capabilities for obtaining structural and dynamic …

Motional broadening: an important distinction between multiple-quantum and satellite-transition MAS NMR of quadrupolar nuclei

SE Ashbrook, S Antonijevic, AJ Berry… - Chemical physics letters, 2002 - Elsevier
Multiple-quantum (MQ) and satellite-transition (ST) magic-angle spinning (MAS) are two
very similar techniques used to obtain high-resolution or 'isotropic'NMR spectra of half …

[PDF][PDF] Quadrupolar nuclei in solid-state nuclear magnetic resonance

D Freude - Encyclopedia of analytical chemistry, 2000 - academia.edu
2 nuclei have been adapted for use with quadrupolar nuclei, and some techniques, eg
double-rotation (DOR) and multiple-quantum transition in combination with fast spinning …

2H Solid-State NMR of Mobile Protons:  It Is Not Always the Simple Way

YJ Lee, T Murakhtina, D Sebastiani… - Journal of the American …, 2007 - ACS Publications
A combined study of 2H line-shape analysis and ab initio molecular dynamics simulations
was carried out on poly [vinyl phosphonic acid](a water-free proton conducting material). We …

Recent advances in solid‐state MAS NMR methodology for probing structure and dynamics in polymeric and supramolecular systems

SP Brown - Macromolecular rapid communications, 2009 - Wiley Online Library
This article reviews recent applications of novel 1H, 2H, 13C, 15N and 17O solid‐state MAS
NMR methods that provide new insight into the structural and dynamic processes that …

Deuterated peptides and proteins in MAS solid-state NMR

M Hologne, V Chevelkov, B Reif - Progress in Nuclear Magnetic …, 2006 - Elsevier
Structure investigations of biological solids by high resolution MAS solid-state NMR have
rapidly progressed the last few years. These investigations recently resulted in the complete …

2H double-quantum MAS NMR spectroscopy as a probe of dynamics on the microsecond timescale in solids

M Cutajar, SE Ashbrook, S Wimperis - Chemical physics letters, 2006 - Elsevier
The sidebands observed in the magic angle spinning (MAS) NMR spectrum of a spin I= 1 2H
nucleus may be very strongly broadened if motion is present in the solid. The broadening …

Localization of vacancies and mobility of lithium ions in Li2ZrO3 as obtained by 6, 7Li NMR

YV Baklanova, IY Arapova, AL Buzlukov… - Journal of Solid State …, 2013 - Elsevier
The 6, 7 Li NMR spectra and the 7 Li spin–lattice relaxation rate were measured on
polycrystalline samples of Li 2 ZrO 3, synthesized at 1050 K and 1300 K. The 7 Li NMR lines …

Order parameters based on 13C1H, 13C1H2 and 13C1H3 heteronuclear dipolar powder patterns: a comparison of MAS‐based solid‐state NMR sequences

J Lorieau, AE McDermott - Magnetic Resonance in Chemistry, 2006 - Wiley Online Library
Order parameters describing conformational exchange processes on the nanosecond to
microsecond timescale can be obtained from powder patterns in solid‐state NMR (SSNMR) …