Recent advances in application of 27Al NMR spectroscopy to materials science

M Haouas, F Taulelle, C Martineau - Progress in nuclear magnetic …, 2016 - Elsevier
Valuable information about the local environment of the aluminum nucleus can be obtained
through 27 Al Nuclear Magnetic Resonance (NMR) parameters like the isotropic chemical …

[HTML][HTML] Advanced solid-state NMR spectroscopy and its applications in zeolite chemistry

M Zheng, Y Chu, Q Wang, Y Wang, J Xu… - Progress in Nuclear …, 2023 - Elsevier
Solid-state NMR spectroscopy (ssNMR) can provide details about the structure, host-
guest/guest-guest interactions and dynamic behavior of materials at atomic length scales. A …

Boron speciation in soda‐lime borosilicate glasses containing zirconium

F Angeli, T Charpentier, D De Ligny… - Journal of the …, 2010 - Wiley Online Library
Boron speciation was investigated in soda‐lime borosilicate glass containing zirconium. In
such compositions, competition between charge compensators (here, sodium and calcium) …

Zero Thermal Expansion in ZrMgMo3O12: NMR Crystallography Reveals Origins of Thermoelastic Properties

CP Romao, FA Perras, U Werner-Zwanziger… - Chemistry of …, 2015 - ACS Publications
The coefficient of thermal expansion of ZrMgMo3O12 has been measured and was found to
be extremely close to zero over a wide temperature range including room temperature (α …

Pure isotropic proton solid state NMR

P Moutzouri, B Simões de Almeida… - Journal of the …, 2021 - ACS Publications
Resolution in proton solid state magic angle sample spinning (MAS) NMR is limited by the
intrinsically imperfect nature of coherent averaging induced by either MAS or multiple pulse …

Synthesis-enabled exploration of chiral and polar multivalent quaternary sulfides

G Akopov, NW Hewage, P Yox, G Viswanathan… - Chemical …, 2021 - pubs.rsc.org
An innovative method of synthesis is reported for the large and diverse (RE) 6 (TM) x (Tt)
2S14 (RE= rare-earth, TM= transition metals, Tt= Si, Ge, and Sn) family of compounds (∼ …

Solid-State NMR of the Family of Positive Electrode Materials Li2Ru1–ySnyO3 for Lithium-Ion Batteries

E Salager, V Sarou-Kanian, M Sathiya… - Chemistry of …, 2014 - ACS Publications
The possibilities offered by ex situ and in situ operando 7Li solid-state nuclear magnetic
resonance (NMR) are explored for the Li2Ru1–y Sn y O3 family (0< y< 1), shown previously …

Structural Modeling of O/F Correlated Disorder in TaOF3 and NbOF3–x(OH)x by Coupling Solid-State NMR and DFT Calculations

O Zakary, M Body, T Charpentier… - Inorganic …, 2023 - ACS Publications
The structure of MOF3 (M= Nb, Ta) compounds was precisely modeled by combining
powder X-ray diffraction, solid-state NMR spectroscopy, and semiempirical dispersion …

Structural characterisation of aluminium layered double hydroxides by 27Al solid-state NMR

A Vyalikh, D Massiot, U Scheler - Solid State Nuclear Magnetic Resonance, 2009 - Elsevier
27Al solid-state NMR has been applied to study the local structure of pristine and chemically
modified aluminium layered double hydroxides (LDH). The pristine LDH only shows six-fold …

Signal enhancement in solid-state NMR of quadrupolar nuclei

FA Perras, J Viger-Gravel, KMN Burgess… - Solid State Nuclear …, 2013 - Elsevier
Recent progress in the development and application of signal enhancement methods for
NMR of quadrupolar nuclei in solids is presented. First, various pulse schemes for …