Characterisation of particles in solution–a perspective on light scattering and comparative technologies

CM Maguire, M Rösslein, P Wick… - … and technology of …, 2018 - Taylor & Francis
We present here a perspective detailing the current state-of-the-art technologies for the
characterisation of nanoparticles (NPs) in liquid suspension. We detail the technologies …

A practical guide to analytical method validation, including measurement uncertainty and accuracy profiles

AG González, MÁ Herrador - TrAC Trends in Analytical Chemistry, 2007 - Elsevier
The objective of analytical method validation is to ensure that every future measurement in
routine analysis will be close enough to the unknown true value for the content of the analyte …

Determination of multi-class pesticides in wines by solid-phase extraction and liquid chromatography-tandem mass spectrometry

A Economou, H Botitsi, S Antoniou, D Tsipi - Journal of chromatography A, 2009 - Elsevier
This work reports a new sensitive multi-residue liquid chromatography-tandem mass
spectrometry (LC-MS/MS) method for detection, confirmation and quantification of forty-six …

Development, validation and application of a LC-MS/MS method for quantification of 15 cannabinoids in food

N Christinat, MC Savoy, P Mottier - Food Chemistry, 2020 - Elsevier
In this study, the occurrence of cannabinoids in hemp-based food products was investigated.
For that purpose, a new liquid chromatography tandem mass spectrometry method for the …

Determination of 76 pharmaceutical drugs by liquid chromatography–tandem mass spectrometry in slaughterhouse wastewater

B Shao, D Chen, J Zhang, Y Wu, C Sun - Journal of Chromatography A, 2009 - Elsevier
A multi-residue method for the analysis of 76 pharmaceutical agents of nine classes of drugs
(tetracyclines, macrolides, fluoroquinolones, β-agonists, β-blockers, diuretics, sedatives …

Bottom-up evaluation of the uncertainty of the quantification of microplastics contamination in sediment samples

V Morgado, C Palma… - … Science & Technology, 2022 - ACS Publications
The quantification and comparison of microplastic contamination of sediments are affected
by sample heterogeneity and the systematic and random effects affecting sample analysis …

Intra-laboratory assessment of method accuracy (trueness and precision) by using validation standards

AG González, MÁ Herrador, AG Asuero - Talanta, 2010 - Elsevier
Assessment of accuracy of analytical methods is a fundamental stage in method validation.
The use of validation standards enables the assessment of both trueness and precision of …

Trends in quality in the analytical laboratory. I. Traceability and measurement uncertainty of analytical results

I Taverniers, M De Loose, E Van Bockstaele - TrAC Trends in Analytical …, 2004 - Elsevier
Credibility of analytical data has never caught the public's eye more than today. The key
principle for quality and reliability of results is comparability between laboratories and on a …

Development and validation of an integrated microfluidic device with an in-line Surface Enhanced Raman Spectroscopy (SERS) detection of glyphosate in drinking …

G Emonds-Alt, C Malherbe, A Kasemiire, HT Avohou… - Talanta, 2022 - Elsevier
Glyphosate, also known as N-(phosphonomethyl) glycine, is one of the most widely used
herbicides in the world. However, the controversy surrounding the toxicity of glyphosate and …

Validation of analytical methods

R Boqué, A Maroto, J Riu… - Grasas y …, 2002 - grasasyaceites.revistas.csic.es
In this paper we shall discuss the concept of method validation, describe the various
elements and explain its close relationship with fitness for purpose. Method validation is …