3D-Printable centrifugal devices for biomolecular solid state NMR rotors
TMO Popp, BT Matchett, RG Green, I Chhabra… - Journal of Magnetic …, 2023 - Elsevier
The advent of magic angle spinning (MAS) rates exceeding 100 kHz has facilitated the
acquisition of 1 H-detected solid-state NMR spectra of biomolecules with high resolution …
acquisition of 1 H-detected solid-state NMR spectra of biomolecules with high resolution …
[HTML][HTML] Setting the magic angle using single crystal sapphire rotors
To date, the most common method for setting the magic angle in magic angle spinning
(MAS) solid state NMR experiments has been to monitor the NMR signal from a quadrupolar …
(MAS) solid state NMR experiments has been to monitor the NMR signal from a quadrupolar …
[HTML][HTML] Improving the sensitivity of MAS spheres using a 9.5 mm spherical shell with 219 μL sample volume spinning in a spherical solenoid coil
C Gao, PH Chen, A Däpp, MA Urban… - Journal of Magnetic …, 2022 - Elsevier
Spherical rotors in magic angle spinning (MAS) nuclear magnetic resonance (NMR)
experiments have potential advantages relative to cylindrical rotors in terms of ease of …
experiments have potential advantages relative to cylindrical rotors in terms of ease of …
Cryogenic-compatible spherical rotors and stators for magic angle spinning dynamic nuclear polarization
Cryogenic magic-angle spinning (MAS) is a standard technique utilized for Dynamic Nuclear
Polarization (DNP) in solid state nuclear magnetic resonance (NMR). Here we describe the …
Polarization (DNP) in solid state nuclear magnetic resonance (NMR). Here we describe the …