Solid‐state NMR spectroscopic methods in chemistry

DD Laws, HML Bitter, A Jerschow - Angewandte Chemie …, 2002 - Wiley Online Library
Over the last decades, NMR spectroscopy has grown into an indispensable tool for chemical
analysis, structure determination, and the study of dynamics in organic, inorganic, and …

[HTML][HTML] Advanced solid-state NMR spectroscopy and its applications in zeolite chemistry

M Zheng, Y Chu, Q Wang, Y Wang, J Xu… - Progress in Nuclear …, 2024 - Elsevier
Solid-state NMR spectroscopy (ssNMR) can provide details about the structure, host–
guest/guest–guest interactions and dynamic behavior of materials at atomic length scales. A …

Advantages of double frequency sweeps in static, MAS and MQMAS NMR of spin I= 3/2 nuclei

APM Kentgens, R Verhagen - Chemical Physics Letters, 1999 - Elsevier
The use of double frequency sweeps (DFSs) consisting of two sidebands generated by a
time-dependent amplitude modulation of the rf-carrier frequency is demonstrated in NMR …

[HTML][HTML] Enhanced room-temperature Na+ ionic conductivity in Na4. 92Y0. 92Zr0. 08Si4O12

A Yang, K Yao, M Schaller, E Dashjav, H Li, S Zhao… - eScience, 2023 - Elsevier
Developing cost-effective and reliable solid-state sodium batteries with superior
performance is crucial for stationary energy storage. A key component in facilitating their …

29Si, 27Al, 1H and 23Na MAS NMR Study of the Bonding Character in Aluminosilicate Inorganic Polymers

MR Rowles, JV Hanna, KJ Pike, ME Smith… - Applied Magnetic …, 2007 - Springer
29 Si, 27 Al, 1 H and 23 Na solid-state magic-angle spinning (MAS) nuclear magnetic
resonance (NMR) has been used to relate nominal composition, bonding character and …

From nuclear structure to the quadrupolar NMR interaction and high-resolution spectroscopy

A Jerschow - Progress in Nuclear Magnetic Resonance …, 2005 - Elsevier
NMR spectroscopy of isotopes with nuclear spin quantum numbers greater than 1/2 has
received wide popularity recently due to the development of powerful high-resolution …

Recent advances in solid-state NMR spectroscopy of quadrupolar nuclei

SE Ashbrook - Physical Chemistry Chemical Physics, 2009 - pubs.rsc.org
Nuclear magnetic resonance (NMR) spectroscopy of quadrupolar nuclei (ie, those with a
spin quantum number I> 1/2) has always been viewed as “difficult” owing to the presence of …

Nucleation and growth of zeolites and inorganic mesoporous solids: Molecular insights from magnetic resonance spectroscopy

JD Epping, BF Chmelka - Current opinion in colloid & interface science, 2006 - Elsevier
Inorganic nano-and mesoporous materials can be prepared with a variety of compositions,
structures, and macroscopic morphologies. Due to their wide range of properties and …

Dipolar recoupling in fast-MAS solid-state NMR spectroscopy

I Schnell - Progress in Nuclear Magnetic Resonance …, 2004 - Elsevier
In view of the success of high-resolution NMR [1–6], in particular recalling the Nobel prizes
awarded to Ernst [7] and Wüthrich [8], one might be tempted to say that solid-state NMR …

High-resolution NMR of quadrupolar nuclei in solids: the satellite-transition magic angle spinning (STMAS) experiment

SE Ashbrook, S Wimperis - Progress in Nuclear Magnetic Resonance …, 2004 - Elsevier
1. Introduction............................................................................. 54 2. Theoretical
background.................................................................... 55 2.1. Origin of quadrupolar …