Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …

In recent years many efforts have been devoted to the screening and the study of new solid-
state forms of old active pharmaceutical ingredients (APIs) with salification or co …

This article reviews the large increase in applications of high-resolution 1H magic-angle
spinning (MAS) solid-state NMR, in particular two-dimensional heteronuclear and …

In spite of tremendous progress made in pulse sequence designs and sophisticated
hardware developments, methods to improve sensitivity and resolution in solid-state NMR …

We describe the encapsulation of mobile proton carriers into defect sites in nonporous
coordination polymers (CPs). The proton carriers were encapsulated with high mobility and …

Dynamic nuclear polarization (DNP), a means of transferring spin polarization from electrons
to nuclei, can enhance the nuclear spin polarization (hence the NMR sensitivity) in bulk …

Understanding hydrogen-bonding networks in nanocrystals and microcrystals that are too
small for X-ray diffractometry is a challenge. Although electron diffraction (ED) or electron 3D …

Fast magic angle spinning (MAS) and proton detection has found widespread application to
enhance the sensitivity of solid-state NMR experiments with spin-1/2 nuclei such as 13 C, 15 …

Cocrystals and amorphous solid dispersions have generated interest in the pharmaceutical
industry as an alternative to more established solid delivery forms. The identification of …

Hexagonal boron nitride nanosheets (h-BNNS), the isoelectronic analog to graphene, have
received interest over the past decade due to their high thermal oxidative resistance, high …